GCMS analysis results for sample AD29669, Jan 2002

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Library Search Compound Report

Data File : M:\INSTRU~l\209\DATA\DEC1301\29669.D Vial: 23 Acq On : 14 Dec 2001 6:22 am Operator: 209 GALOS Sample : gems scan 12/7 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.43 0.45 ug/1 169801 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1- -methoxy-1-methylet 148 C7H16O3 020324-32-7 72

A 2 2-Butanol, 3,3 1 -oxybis- 162 C8H18O3 054305-61-2 50 3 Ether / 74 C4H10O 000060-29-7 42 4 1-Propanol, 2-(2-hydroxypropoxy) - 134 C6H14O3 000106-62-7 42 'Abundance Scan 696 (11.431 min): 29669.D (-) m/z 59.05 100.00% K 9

45 5000 73 103 11.20 11.40 11.60 11.80 I | — ... .. 66 .86 94........ m/z 45.00 51.08% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 'Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 103 45 11.20 11 40 11.60 11.80 73 31 m/z 102.95 33 . 22% ! ------- ■ i ■ ■ ' ‘ i ■ • ■ ■ i ' ......... ,...... ,130... m/Z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3‘-oxybis- 59 GGEEuu I . I » i I I fl 11.20 11.40 11.60 11.80 5000 31 45 m/z 73.00 28.31% 103

mlz-> 'Abundance 31 I ______. i______ l !________ \______ 1 । • 1 1 * r* ' * 1 । ’ 1 1 1 । • 1 ’ 1 । 20 30 40 50 60 • 1 । 70 80 ........... '............ 134 , 90 #62576: Ether 100 110 120 130 140 _M) m/z 11.20 41 05 11.40 11.60 11.80 22.23% 59 5000 45 74

m/z-> 20 30 40 । । ■ । 50 • l ■ • ■ ■ । ■ 60 70 80 90 100 110 120 130 140 _।W w 11.20 11.40 11.60 11.80

29669.D GCMS1126.M Tue Jan 08 11:00:06 2002 Page 2

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