GCMS analysis results for sample AD29734, Jan 2002

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Library Search Compound Report

Data File : M:\INSTRU~1\209\DATA\DEC1301\29734.D Vial: 20 Acq On : 14 Dec 2001 3:26 am Operator: 209 GALOS Sample : gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 2-Propanol, 1-(2-methoxy-1-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.42 0.49 ug/1 173486 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-me oxy-1-methylet 148 C7H16O3 020324-32-7 83 2 2-Butanol, 3,3'-oxy is- 162 C8H18O3 054305-61-2 50 3 2-Propanol, 1, I' 1 -xybis- 134 C6H14O3 000110-98-5 50 4 1-Propanol, 2- (/-hydroxypropoxy)- 134 C6H14O3 000106-62-7 42 Abundance / Scan 695 (11.422 min): 29734.D (-) m/z 59.05 100.00% $

5000 45 73 103 . MU. X 11.00 11.20 11 40 11.60 11.80 39 ----- 85...... ।................. m/z 44.95 52.05% m/z-? 20 30 40 50 60 70 80 90 00 110 120 130 140 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 45 103 11.00 11.20 11.40 11.60 11.80 73 31 m/z 103.00 36.91% ........... ।.......... 130.... - T ----- m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol. 3,3’-oxybis- 59

11.00 11.20 11.40 11.60 11.80 5000 31 45 m/ z 73.00 30.68% 103

. I l . l. I .... .134 > । ■ > • > । > • i ■ ■ • • i ■ ' i ' ' ■ ' i ' ’ i ' ' ' ——————— m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6087: 2-Propanol, 1,1'-oxybis- 59 11.00 11.20 11.40 11.60 11.80 m/ z 41.05 28.00% 31 5000 45

- — I । । । I 72 89 I 103

' ' I ' ' '' t 111‘I 1 '' ' I ■ i ■ • i ■ ■ ■ ■ i • ■ ■ • i ■ ■ > ■ l ■ J A m/z-> 20 30 40 50 (60 70 80 90 100 110 120 130 140 11 00 11.20 11.40 11.60 11.80

29734.D GCMS1126.M Tue Jan 08 11:04:28 2002 Page 3

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