GCMS analysis results for sample AD29671, Jan 2002

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Library Search Compound Report

Data File : M:\INSTRU~l\209\DATA\DEC1301\29671.D Vial: 18 Acq On : 14 Dec 2001 1:29 am Operator: 209 GALOS Sample : gems scan 12/7 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 2-Propanol, 1,I'-oxybis- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.42 1.05 ug/1 371865 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1,1‘- oxybi s- 134 C6H14O3 000110-98-5 56 2 2-Propanol, l -(2-methoxypropoxy) - 148 C7H16O3 013429-07-7 40 3 2-Butanol, 3 /3 ' -oxybis- 162 C8H18O3 054305-61-2 39 4 2 -Propanol,2 1-(2-methoxy-1-methylet 148 C7H16O3 _______ 020324-32-7 39 Abundance / Scan 694 (11.419 min): 29671.D (-) m/z 59.05 100.00% 59

miz-> 5000

0-1 20 — 30 2l51l 40 50 — 60 45

TT 70 73

80 85... .......... 90 100 103

110 120 130 140 11.00 11.20 11.40 11.60 11.80 m/z M 44.9.5 46.68% 1t"

Abundance #6087: 2-Propanol, 1,1-oxybis- 59 31 5000- 45 J i 1 Tr i 1 1 ‘ ‘ I 1 1 ' ■ I ' ' 11.00 11.20 11.40 11.60 11.80 103 m/ Z 10 3.0.5 33.63%

miz-> ............. ........... — 20 30 40 -2... _ 50 60 70 80 90 100 110 120 130 140 Abundance #9233: 2-Propanol, 1-(2-methoxypropoxy)- 59

11.00 11.20 11.40 11.60 11.80 5000 m/z 73.00 30.18%

m/z-> Abundance 20 31

40 45 ! ' ' I ' ' ' ' I ' ' ' ' I ' ’ ' ' I ' ' ' ' I ' ' ' ' 1‘‘31r (-> , t-r-j- r-TT-rTn-rT-T-j-rT-rT-p-rrnr-p-, TIit 30 50 60 #12859: 2-Butanol, 3,3'-oxybis- 59 70 73 l 80 90 100 104 110 120 130 130 140

m/z . NA 11.00 11.20 11.40 11.60 11.80 | 41.05 24.30%

m/z-> 5000

-IP 4 ■ i ■ 20 30 40 50 31 45

11 60 70 80 90 103

............................... 134 100 110 120 130 140 —TP V 11.00 11.20 11.40 11.60 11.80

29671.D GCMS1126.M Tue Jan 08 11:03:06 2002 Page 3

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