GCMS analysis results for sample AD29668, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : M:\INSTRU~1\209\DATA\DEC1301\29668.D Vial: 22 Acq On : 14 Dec 2001 5:24 am Operator: 209 GALOS Sample : gems scan 12/7 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.43 0.41 ug/1 138410 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative I MW MolForm CAS# Qual

1 2-Propanol, 1- (2-methoxy-1-methylet 148 C7H16O3 020324-32-7 83 2 2-Propanol, 1- (2 -methoxypropoxy) - 148 C7H16O3 013429-07-7 50 3 2-Butanol, 3,3' -oxybis- 162 C8H18O3 054305-61-2 45 4 1-Propanol, 2-(2/hydroxypropoxy)- 134 C6H14O3 000106-62-7 42 Abundance Scan 696 (11.432 min): 29668.D (-) m/z 59.05 100.00% 59

5000 45

73 103 N i m/z-> Abundance

miz-> Abundance 5000

----------- 20 30 20

40 30

31 - 40

45 50

50 +44..... + 60 #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

60 70

70 80

73 90 86...... ।................. 100 110 120

103

........... ।.......... 130.... 80 90 100 110 120 130 140 #9233: 2-Propanol, 1-(2-methoxypropoxy)- 130 140 m/z

N 11.20 11.40 11.60 11.80 45.00

11.20 11.40 11.60 11.80 .m/z 102.95 4 9.91%

35.63%

! 59 TIf 11.20 11.40 11.60 11.80 5000 m/z 41.05 30.00%

31 45 73 ■ i ' ' • ■ i ■ •I 1 I ' ' ' ' I ■ '' ' i ' ' ' ' I ' _ 194......... 130 m/z-> 20 30 40 50 60 70 80, .90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3'-oxybis- 59 11.20 11.40 11.60 11.80 m/z 73.00 7.69%

M 5000 - 31 45 103

134 -PP . , , । 4 — •f-r-r-r-r-r-.-r ri । 1———— TT rp-n i rrrrTyrrrrj-r m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 11.20 11.40 11.60 11.80

29668.D GCMS1126.M Tue Jan 08 10:58:58 2002 Page 3

NYC-WTC_000036900