GCMS analysis report for sample AD30488 showing detection of unknown compounds and surrogate recovery data from February 8, 2002.
NYC-WTC_000018882–000018897Folder label: “GCMS X 12/17/01 A 12/22 - 12/23/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\DEC2701\30488.D Vial: 16 Acq On : 29 Dec 2001 1:48 pm Operator: 209 GALOS Sample : GC/MS SCAN Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 7.75 0.69 ug/1 237699 1,4-Dichlorobenzene-d4 11.67 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2 - Propanone/, 1,1,1 - tri chloro - 160 C3H3C130 000918-00-3 32 2 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 9 3 Propionic acid, 2,2-dichloro-, pent 212 C8H14C12O2 017640-08-3 9 4 Ethyl Chloride 64 C2H5C1 000075-00-3 9 Abundance Scan 295 (7.753 min): 30488.D (-) m/z 43.05 100.00% 43
5000
44t41auuuI । rrrpn'i t। । 35 ,49 56 .63 72 83 97 119125 7.40 7.60 7.80 8.00 •n । rri > । i i i i । i ■am 1 re .Hi d’rti । ] i .‘i । 11'1', ■ । .. .I.',-,, , . ,, 1’ , ,1.1. । , m/z 124.85 9.26% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43
5000 •1***1* 7.40 7.60 7.80 8.00 15 m/z 35.00 7.51% 35 A9 85 97 117 125 ■ ‘ i ■ ■ ■11 • ■ • • i • ' 11' 1 ''I'1 ‘*I*‘*‘I* TIUmuunTmgr miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4732: N-Acetylpyrrolidone 43 » » 1-88 > l iff 8 ’ 1,1 i 1 7.40 7.60 7.80 8.00 5000 m/z 82.8.0 6.83% 99 127 30 56 69 112 — — —— — — • l • • • > । > l • *’144**144**1**3*1’* miz-> Abundance 10 20 30 40 50 60 70 80 90 100 110 120 130 #25703: Proptonic acid, 2,2-dichloro-, pentyl ester MAAAAW/AAAA.A.AA 43 7.40 ' 7.60 ‘ 7.80 ' ' 8.00 ' m/z 81.85 6.82% 71 5000
27 97 . 1111 •'1 • 11 1111 mH 62 90 +tt '111111 ' 1Il ■105 ’’u । 11 11 । । । ।i । । । 1......... M....... ' ' I ‘ ‘ • I ‘ ‘ 1 I ’ 1 1 'P > I I I I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 7,40 7.60 7.80 8.00
30488.D GCMS1126.M Tue Jan 29 14:30:14 2002 Page 2
NYC-WTC_000018890
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NYC-WTC_000018817
Laboratory report of GCMS analysis for sample AD28860 conducted on December 16, 2001, showing compound identification.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018898
GCMS analysis report for sample AD26827 showing detection of unknown compounds and surrogate recovery data from December 21, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017144
Laboratory report documenting GCMS analysis of sample AD30601 including DDD surrogates on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017246
Gas chromatography-mass spectrometry analysis report for sample AD30602 showing detection of 2,4-DDD and other unknown compounds, analyzed January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017171
Laboratory report documenting GCMS analysis of sample AD30607 including DDD surrogates on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017192
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30608 performed on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018923
GCMS analysis report for sample AD26477 showing detection of unknown compounds and surrogate recovery data from December 21, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017299
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30634 performed on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017210
Laboratory report documenting GCMS analysis of sample AD30633 including DDD surrogates on January 22, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018870
GCMS analysis report for sample AD30485 showing detection of unknown compounds and surrogate recovery data from February 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018858
GCMS analysis report for sample AD30606 showing detection of unknown compounds and surrogate recovery data from February 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017233
Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD30603 on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000018795
Single-page document containing GCMS data or metadata associated with the WTC site in late December 2001.
Filed in the same folder
NYC-WTC_000018796
Fragmented GCMS data page containing chemical identifiers and numerical values from a December 2001 analysis.
Filed in the same folder
NYC-WTC_000018799
Calibration report listing response factors and concentrations for multiple organic compounds analyzed on December 22, 2001.
Filed in the same folder
NYC-WTC_000018803
Reference data report showing measured versus expected values for organic compounds in sample AD29735.
Filed in the same folder
NYC-WTC_000018808
Blank analysis report confirming no detectable levels of target compounds above the method detection limit.
Filed in the same folder