GCMS analysis log for sample AD31017

NYC 9/11 Public Portal Document . Quantitation Report (QT Reviewed) » * +‘ fata File : C:\HPCHEM\1\DATA\JAN0802\REF.D Vial: 8 -' Aeq On : 8 dan 2002 8:10 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 8 20:59 2002 Quant Results File: GCMS0103.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update +: Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103 Internal Standards R.T. Qlon Response Conc Units Dev (Min) 1) 1,4-Dichlorobenzene-d4 11.53 152 828358 20.00 ug/l 0.00 10) Naphthalene-de 15.13 136 3179098 20.00 ug/l 0.00 17) Acenaphthene-d10 20.39 164 1539688 20.00 ug/l 0.00 29) Phenanthrene-d10 24.80 188 2218237 20.00 ug/l 0.00 38) Chrysene-d12 32.84 240 1249289 20.00 ug/1 0.00 44) Perylene-d12 36.90 264 721104 20.00 ug/1 0.00 System Monitoring Compounds 37) 2,4-DDD 29.88 235 126371 4.96 ug/ml -0.19 Spiked Amount 5.000 Recovery = 99.20% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.29 74 80653 2.03 ug/l 90 3) bis (2-Chloroethyl) ether 10.96 93 192652 3.00 ug/1 99 4) 1,3-Dichlorobenzene 11.43 146 126999 2.21 ug/l 95 5) 1,4-Dichlorobenzene 11.58 146 140968 2.44 ug/1 97 6) 1,2-Dichlorobenzene 12.08 146 139863 2.62 ug/l 98 7) 2,2'-oxybis(1-Chloropropan 12.43 45 328624 3.44 ug/l 95 8) N-Nitroso-di-n-propylamine 12.81 70 137665 3.44 ug/l 99 9) Hexachloroethane 12.92 117 38613 1.63 ug/1 95 11) Nitrobenzene 13.20 77 176397 2.87 ug/1 93 12) Isophorone 13.85 82 381986 3.49 ug/l 99 13) bis(2-Chloroethoxy)methane 14.54 93 246799 3.48 ug/L 100 14) 1,2,4-Trichlorobenzene 15.02 180 114025 2.63 ug/l 96 15) Naphthalene 15.18 128 486036 3.34 ug/1 99 16) Hexachlorobutadiene 15.73 225 33335 1.52 ug/L 97 18) Hexachlorocyclopentadiene 17.92 237 539 N.D. 19) 2-Chloronaphthalene 18.66 162 - 278018 3.49 ug/l 99 20) Dimethylphthalate 19.78 163 394153 4.22 ug/1 99 21) 2,6-Dinitrotoluene 19.99 165 65292 2.95 ug/l 98 22) Acenaphthylene 19.92 152 414059 3.52 ug/l 99 23) Acenaphthene 20.48 153 325276 4.03 ug/l 99 24) 2,4-Dinitrotoluene 21.16 165 77351 2.73 ug/l # 93 25) Diethylphthalate 21.91 149 407346 4.39 ug/1 100 26) 4-Chlorophenyl-phenylether 22.03 204 161779 4.30 ug/l 96 27) Fluorene 21.99 166 347217 4.24 ug/1 98 28) Azobenzen/ 1,2-Diphenylhyd 22.50 77 403925 3.68 ug/L 98 (#) = qualifier out of range (m) = manual integration REF.D GCMS0103.M Wed Jan 09 12:46:26 2002 Page 1 NYC-WTC_000017341 :