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GCMS analysis log for sample AD31017

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31017 performed on January 18, 2002.

NYC-WTC_000017338–000017343

Folder label: “GCMS X 12/20/01 A 1/8/02

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NYC 9/11 Public Portal Document . Quantitation Report (QI Reviewed) ‘ +" fata File : C:\HPCHEM\1\DATA\JAN0802\REF.D Vial: 8 + Aeq On : 8 Jan 2002 8:10 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 8 20:59 2002 Quant Results File: GCMS0103.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update +: Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103 Compound R.T. QIon Response Conc Unit Qvalue 30) N-Nitrosodiphenylamine 22.44 168 112765 3.10 ug/1 97 31) 4-Bromophenyl-phenylether 23.49 248 81839 3.96 ug/l 95 32) Hexachlorobenzene 23.90 284 95873 4.01 ug/l 98 33) Phenanthrene 24.87 178 482855 4.29 ug/l 99 34) Anthracene 25.01 178 426878 3.88 ug/l 99 35) Di-n-butylphthalate 26.83 149 611758 4.02 ug/l 99 36) Fluoranthene 28.48 202 433277 4.02 ug/1 98 39) Pyrene 29.15 202 456029 4.11 ug/l 97 40) Butylbenzylphthalate 31.33 149 197866 3.29 ug/1 98 41) Benzo(a) anthracene 32.78 228 273125 3.91 ug/l 99 42) Bis(2-ethylhexyl)phthalate 33.13 149 264520 3.25 ug/l 99 43) Chrysene 32.91 228 302803 4.40 ug/1 98 45) Di-n-Octylphthalate 34.87 149 212137 1.83 ug/l # 94 46) Benzo (b) fluoranthene 35.86 252 195984 3.28 ug/1 98 47) Benzo (k) fluoranthene 35.92 252 241591 4,11 ug/1 99 48) Benzo(a)pyrene 36.73 252 148451 3.17 ug/1 97 49) Indeno(1,2,3-cd) pyrene 40.48 276 151842 3.44 ug/1 98 50) Dibenz(a,h) anthracene 40.53 278 132756 3.92 ug/l 98 51) Benzo(g,h,i)perylene 41.53 276 137391 3.72 ug/1 99 (#) = qualifier out of range (m) = manual imtegration REF.D GCMS0103.M Wed Jan 09 12:46:29 2002 Page 2 NYC-WTC_000017342

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NYC-WTC_000017342Source: NYC Law Department, mirrored locally

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