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GCMS reference data for volatile organics, Jan 2002

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Reference data sheet from the DEP laboratory documenting GCMS analysis parameters and results for volatile organic compounds.

NYC-WTC_000016916–000016920

Folder label: “GCMS X 12/24/01 A 1/10/02

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NYC 9/11 Public Portal Document . Quantitation Report (QT Reviewed) . Data File : C:\HPCHEM\1\DATA\JAN0902\REF.D Vial: 5 Acq On : 10 Jan 2002 7:26 pm Operator: 209 GALOS Sample : gems scan 12/24 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 5 16:27 2002 Quant Results File: GCMS0103.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Dec 13 14:40:46 2001 Response via : Initial Calibration DataAcg Meth : GCMS0103 Compound R.T. QIon Response Conc Unit Qvalue 30) N-Nitrosodiphenylamine 22.43 168 103031 3.70 ug/1 99 31) 4-Bromophenyl-phenylether 23.49 248 61200 3.87 ug/l 99 32) Hexachlorobenzene 23.91 284 68703 3.75 ug/l 98 33) Phenanthrene 24.87 178 367133 4.27 ug/l 99 34) Anthracene 25.00 178 335217 3.98 ug/1 99 35) Di-n-butylphthalate 26.83 149 497209 4.26 ug/1 99 36) Fluoranthene 28.48 202 340677 4.13 ug/l 98 39) Pyrene 29.15 202 353736 4.00 ug/l 94 40) Butylbenzylphthalate 31.33 149 155827 3.25 ug/l 99 41) Benzo(a) anthracene 32.78 228 226809 4.07 ug/1 98 42) Bis(2-ethylhexyl)phthalate 33.13 149 197318 3.04 ug/l 98 43) Chrysene 32.90 228 250034 4.56 ug/l 99 45) Di-n-Octylphthalate 34.88 149 184475 2.02 ug/l # 96 46) Benzo(b) fluoranthene 35.86 252 162290 3.46 ug/1 99 47) Benzo(k) fluoranthene 35.92 252 214149 4.64 ug/l 99 48) Benzo(a)pyrene 36.73 252 123690 3.37 ug/l 97 49) Indeno(1,2,3-cd) pyrene 40.49 276 116211 3.35 ug/l 99 50) Dibenz(a,h) anthracene 40.55 278 100718 3.79 ug/l 99 51) Benzo(g,h,i)perylene 41.53 276 108858 3.76 ug/l 98 (#) = qualifier out of range (m) = manual integration REF.D GCMS0103.M Tue Feb 05 16:30:22 2002 Page 2 NYC-WTC_000016919

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NYC-WTC_000016919Source: NYC Law Department, mirrored locally

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