GCMS reference data for volatile organics, Jan 2002

NYC 9/11 Public Portal Document : Quantitation Report (QT Reviewed, : Data File : C:\HPCHEM\1\DATA\JAN0902\REF.D Vial: 5 Acq On : 10 Jan 2002 7:26 pm Operator: 209 GALOS Sample : gems scan 12/24 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 5 16:27 2002 Quant Results File: GCMS0103.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator, Title : 209 625/TCLP calibration table Last Update : Thu Dec 13 14:40:46 2001 Response via : Initial Calibration DataAcg Meth : GCMS0103 Internal Standards R.T. Qlon Response Conc Units Dev (Min! 1) 1,4-Dichlorobenzene-d4 11.53 152 589969 20.00 ug/l 0.00 10) Naphthalene-ds 15.12 136 2316106 20.00 ug/l 0.00 17) Acenaphthene-d10 20.39 164 1175601 20.00 ug/l 0.00 29) Phenanthrene-d10 24.81 188 1698158 20.00 ug/l 0.00 38) Chrysene-d12 32.83 240 995677 20.00 ug/1 0.00 44) Perylene-di2 36.90 264 565841 20.00 ug/1 0.00 System Monitoring Compounds 37) 2,4-DDD 29.88 235 102301 5.25 ug/ml -0.19 Spiked Amount 5.000 Recovery = 105.00% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.30 74 68081m 2.41 ug/l 3) bis (2-Chloroethyl) ether 10.96 93 160162 3.50 ug/1 99 4) 1,3-Dichlorobenzene 11.43 146 100391 2.46 ug/l 99 5) 1,4-Dichlorobenzene 11.57 146 110790m 2.69 ug/l 6) 1,2-Dichlorobenzene 12.08 146 108964 2.87 ug/l 97 7) 2,2'-oxybis(1-Chloropropan 12.43 45 268355 3.95 ug/l 96 8) N-Nitroso-di-n-propylamine 12.81 70 113727 3.99 ug/l 97 9) Hexachloroethane 12.92 117 31800 1.89 ug/l 95 11) Nitrobenzene 13.20 77 146540 3.28 ug/l 99 12) Isophorone 13.85 82 322489 4.04 ug/l 99 13) bis(2-Chloroethoxy) methane 14.54 93 192331 3.72 ug/l 98 14) 1,2,4-Trichlorobenzene 15.02 180 90126 2.86 ug/1 99 15) Naphthalene 15.18 128 380991 3.59 ug/l 99 16) Hexachlorobutadiene 15.74 225 27605 1.73 ug/1 96 18) Hexachlorocyclopentadiene 17.91 237 388 N.D. 19) 2-Chloronaphthalene 18.67 162 209249 3.44 ug/l 99 20) Dimethylphthalate 19.78 163 308201 4.32 ug/l 100 21) 2,6-Dinitrotoluene 19.99 165 48086 2.84 ug/l 95 22) Acenaphthylene 19.92 152 329403 3.67 ug/l 100 23) Acenaphthene 20.48 153 240966 3.91 ug/1 99 24) 2,4-Dinitrotoluene 21.16 165 59943 2.77 ug/1 94 25) Diethylphthalate 21.91 149 315610 4.46 ug/1 99 26) 4-Chlorophenyl-phenylether 22.03 204 114535 3.99 ug/l 97 27) Fluorene 22.00 166 260071 4.16 ug/l 100 28) Azobenzen/ 1,2-Diphenylhyd 22.49 77 307524 3.67 ug/L 97 (#) = qualifier out of range (m) = manual integration REF.D GCMS0103.M Tue Feb 05 16:30:18 2002 Page 1 NYC-WTC_000016918