GCMS reference results, sample AD31129, Jan 2002

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Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\JAN0802\REFD.D Vial: 18 Acq On : 10 Jan 2002 6:23 am Operator: 209 GALOS Sample : gems scan 12/21 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 6 9:09 2002 Quant < Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.53 152 863842 20.00 ug/1 0.00 10) Naphthalene-d8 15.13 136 3346473 20.00 ug/1 0.00 17) Acenaphthene-diO 20.39 164 1666638 20.00 ug/1 0.00 29) Phenanthrene-diO 24.81 188 2401456 20.00 ug/1 0.00 38) Chrysene-dl2 32.84 240 1442178 20.00 ug/1 0.00 44) Perylene-dl2 36.90 264 824112 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 29.89 235 99066 3.59 ug/mL -0.18 Spiked Amount 5.000 Recovery = 71.80%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.29 74 60766 1.47 ug/1 91 3) bis(2-Chloroethyl)ether 10.96 93 159041 2.38 ug/1 95 4) 1,3-Dichlorobenzene 11.44 146 103719 1.73 ug/1 98 5) 1,4-Dichlorobenzene 11.57 146 115343m 1.91 ug/1 6) 1,2-Dichlorobenzene 12.08 146 111627 2.00 ug/1 95 7) 2,2'-oxybis(1-Chloropropan 12.43 45 267528 2.69 ug/1 95 8) N-Nitroso-di-n-propylamine 12.81 70 113095 2.71 ug/1 97 9) Hexachloroethane 12.91 117 35527 1.44 ug/1 94 11) Nitrobenzene 13.21 77 148367 2.30 ug/1 96 12) 1sophorone 13.85 82 319979 2.78 ug/1 99 13) bis(2-Chloroethoxy)methane 14.55 93 193087 2.59 ug/1 98 14) 1,2,4-Trichlorobenzene 15.02 180 95088 2.09 ug/1 99 15) Naphthalene 15.18 128 390307 2.55 ug/1 99 16) Hexachiorobutadiene 15.73 225 33629 1.46 ug/1 99 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 18.66 162 216538 2.51 ug/1 100 20) Dimethylphthalate 19.78 163 296559 2.93 ug/1 99 21) 2,6-Dinitrotoluene 19.99 165 47344 1.97 ug/1 98 2 2) Acenaphthylene 19.92 152 326954 2.57 ug/1 98 23) Ac enapht hene 20.48 153 249760 2.86 ug/1 100 24) 2,4-Dinitrotoluene 21.16 165 58971 1.92 ug/1 91 25) Diethylphthalate 21.91 149 308082 3.07 ug/1 100 26) 4-Chlorophenyl-phenylether 22.04 204 117860 2.89 ug/1 99 27) Fluorene 21.99 166 260298 2.94 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 22.50 77 303969 2.56 ug/L 99

(#) = qualifier out of range (m) = manual integration REFD.D GCMS0103.M Wed Feb 06 09:11:08 2002 Page 1

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