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GCMS calibration report, December 2001

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GCMS calibration report for sample AD30009 dated December 20, 2001, listing standard compound responses.

NYC-WTC_000016807–000016810

Folder label: “GCMS X 12/12/01 A 12/20/01

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NYC 9/11 Public Portal Document - Quantitation Report (QT Reviewed) . Data File : C:\HPCHEM\1\DATA\DEC1901\CAL25A.D Vial: 2 Acq On : 20 Dec 2001 10:13 am Operator: 209 GALOS Sample : Inst : GC/MS 209 Misc e Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 2 10:02 2002 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : NPO91101 Compound R.T. QIon Response Conc Unit Qvalue 30) N-Nitrosodiphenylamine 22.63 168 2184809 25.00 ug/l 94 31) 4-Bromophenyl-phenylether 23.66 248 1232395 25.45 ug/l 96 32) Hexachlorobenzene 24.10 284 1405288 26.39 ug/l 98 33) Phenanthrene 25.07 178 6498868 24,93 ug/l 99 34) Anthracene 25.20 178 6427064 24.74 ug/l 100 _35) Di-n-butylphthalate 27.01 149 8892900 25.64 ug/l 99 36) Fluoranthene 28.68 202 6528195 25.94 ug/1 98 39) Pyrene 29.35 202 6848756 22.50 ug/l 99 40) Butylbenzylphthalate 31.51 149 3589729 22.58 ug/1 91 41) Benzo(a) anthracene 32.98 228 5154031 24.52 ug/l 99 42) Bis(2-ethylhexyl)phthalate 33.30 149 4670658 21.74 ug/1 99 43) Chrysene 33.12 228 4939628 23.97 ug/1 99 45) Di-n-Octylphthalate 35.05 149 7292667 21.71 ug/l # 95 46) Benzo(b) fluoranthene 36.07 252 4932345 25.93 ug/l 99 47) Benzo(k) fluoranthene 36.13 252 4782365 24.50 ug/l 99 48) Benzo(a)pyrene 36.96 252 4047849 24.48 ug/l 100 49) Indeno(1,2,3-cd) pyrene 40.83 276 3974301 24.04 ug/l 97 50) Dibenz(a,h) anthracene 40.90 278 3145648 24.29 ug/l 96 51) Benzo(g,h,i)perylene 41.93 276 3209700 22.72 ug/1 94 (#) = qualifier out of range (m) = manual integration CAL25A.D GCMS1126.M Wed Jan 02 10:04:12 2002 Page 2 NYC-WTC_000016809

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NYC-WTC_000016809Source: NYC Law Department, mirrored locally

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