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GCMS reference analysis results for sample AD29932, Dec 2001

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Reference standard analysis report for gas chromatography-mass spectrometry of sample AD29932 conducted on December 18, 2001.

NYC-WTC_000037239–000037243

Folder label: “GCMS X 12/11/01 A 12/18/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\DEC1801\REF.D Vial: 7 Acq On : 18 Dec 2001 9:56 pm Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 15 9:57 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : NP091101

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.59 168 132079 3.02 ug/1 # 87 31) 4-Bromophenyl-phenylether 23.66 248 79726 3.29 ug/1 92 32) Hexachlorobenzene 24.07 284 94802 3.56 ug/1 96 3 3) Phenanthrene 25.04 178 472493 3.62 ug/1 99 3 4) Anthracene 25.17 178 434143 3.34 ug/1 100 35) Di-n-butylphthalate 26.99 149 600796 3.46 ug/1 99 36) Fluoranthene 28.65 202 434736 3.45 ug/1 95 39) Pyrene 29.32 202 463506 3.17 ug/1 99 40) Butylbenzylphthalate 31.50 149 192466 2.52 ug/1 88 41) Benzo(a)anthracene 32.96 228 334058 3.31 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.30 149 261425 2.54 ug/1 99 43) Chrysene 33.09 228 378144 3.82 ug/1 99 45) Di-n-Octylphthalate 35.03 149 292742 1.87 ug/1 # 90 46) Benzo(b)fluoranthene 36.04 252 309257 3.48 ug/1 97 47) Benzo(k)fluoranthene 36.10 252 346539 3.80 ug/1 99 48) Benzo(a)pyrene 36.93 252 219297 2.84 ug/1 97 49) Indeno(l,2,3-cd)pyrene 40.79 276 216838 2.81 ug/1 95 5 0) Dibenz(a,h)anthracene 40.86 278 177999 2.94 ug/1 95 51) Benzo(g,h,i)perylene 41.88 276 193482 2.93 ug/1 # 89

(#) = qualifier out of range (m) = manual integration REF.D GCMS1126.M Tue Jan 15 09:58:25 2002 Page 2

NYC-WTC_000037242

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NYC-WTC_000037242Source: NYC Law Department, mirrored locally

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