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GCMS reference standard results, Jan 2002

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Reference analysis report for gas chromatography-mass spectrometry quantification of volatile organic compounds conducted on December 29, 2001.

NYC-WTC_000019044–000019048

Folder label: “GCMS X 12/13/01 A 12/22/01 AND 12/27/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC2 7 01\REFA.D Vial: 4 Acq On : 29 Dec 2001 2:07 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 31 11:20 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update ’ : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.60 168 133449 2.96 ug/1 # 31) 4-Bromophenyl-phenylether 23.67 248 99130 3.97 ug/1 # 3 2) Hexachlorobenzene 24.08 284 118535 4.32 ug/1 3 3) Phenanthrene 25.04 178 573074 4.27 ug/1 3 4) Anthracene 25.18 178 512818 3.83 ug/1 35) Di-n-butylphthalate 27.00 149 819074 4.58 ug/1 # 36) Fluoranthene 28.67 202 526851 4.06 ug/1 39) Pyrene 29.33 202 558210 4.15 ug/1 99 40) Butylbenzylphthalate 31.51 149 223773 3.18 ug/1 # 82 41) Benzo(a)anthracene 32.97 228 359064 3.87 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.30 149 294876 3.11 ug/1 97 43) Chrysene 33.09 228 413066 4.54 ug/1 100 45) Di-n-Octylphthalate 35.04 149 301742 2.34 ug/1 # 90 46) Benzo(b)fluoranthene 36.05 252 307039 4.20 ug/1 98 47) Benzo(k)fluoranthene 36.11 252 373464 4.97 ug/1 98 4 8) Benzo(a)pyrene 36.94 252 211315 3.32 ug'/l 97 49) Indeno (1,2,3-cd) pyrene 40.83 276 190137 2.99 ug/1 93 5 0) Dibenz(a,h)anthracene 40.89 278 160247 3.22 ug/1 95 51) Benzo(g,h,i)perylene 41.93 276 181465 3.34 ug/1 94

(#) = qualifier out of range (m) = manual integration REFA.D GCMS1126.M Mon Dec 31 11:20:53 2001 Page 2

NYC-WTC_0000 19047

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NYC-WTC_000019047Source: NYC Law Department, mirrored locally

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