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GCMS reference standard results Dec 2001

Machine-extracted title · confidence 90%

Reference standard analysis report for GCMS testing showing concentrations of target analytes and detection limits.

NYC-WTC_000036345–000036349

Folder label: “GCMS X 12/5/01 A 12/12/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC12 01\REFE.D Vial: 16 Acq On : 12 Dec 2001 5:37 pm Operator: 209 GALOS Sample : gc/ms scan 12/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 12 18:26 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.59 168 87724 1.88 ug/1 # 92 31) 4-Bromophenyl-phenylether 23.66 248 76430 2.95 ug/1 97 3 2) Hexachlorobenzene 24.07 284 83273 2.92 ug/1 99 3 3) Phenanthrene 25.04 178 440061 3.16 ug/1 99 34) Anthracene 25.17 178 380766 2.74 ug/1 99 35) Di-n-butylphthalate 26.98 149 568917 3.07 ug/1 # 98 36) Fluoranthene 28.65 202 413758 3.08 ug/1 99 3 9) Pyrene 29.31 202 427522 2.90 ug/1 99 40) Butylbenzylphthalate 31.49 149 182710 2.37 ug/1 91 41) Benzo(a)anthracene 32.96 228 306698 3.01 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.29 149 277182 2.66 ug/1 100 43) Chrysene 33.0. 228 335343 3.36 ug/1 99 45) Di-n-Octylphthalate 35.03 149 274633 1.72 ug/1 # 91 4 6) Benzo(b)fluoranthene 36.03 252 273751 3.03 ug/1 99 47) Benzo(k)fluoranthene 36.10 252 316539 3.41 ug/1 99 48) Benzo(a)pyrene 36.92 252 187713 2.39 ug/1 98 49) Indeno(1,2,3-cd)pyrene 40.77 276 197524 2.51 ug/1 93 50) Dibenz(a,h)anthracene 40.83 278 165853 2.70 ug/1 97 51) Benzo(g,h,i)perylene 41.86 276 176651 2.63 ug/1 94

(#) = qualifier out of range (m) = manual integration REFE.D GCMS1126.M Fri Dec 21 12:41:01 2001 Page 2

NYC-WTC_000036348

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NYC-WTC_000036348Source: NYC Law Department, mirrored locally

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