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GCMS calibration report, Dec 2001

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Calibration data for GCMS analysis of volatile organic compounds dated December 6, 2001.

NYC-WTC_000035439–000035443

Folder label: “GCMS X 11/27/01 A 12/7/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC0601\REFA.D Vial: 26 Acq On : 7 Dec 2001 12:04 am Operator: 209 GALOS Sample : 11/27 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 7 15:45 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.59 168 159882 3.25 ug/1 97 31) 4-Bromophenyl-phenylether 23.66 248 95007 3.49 ug/1 97 32) Hexachlorobenzene 24.07 284 106382 3.55 ug/1 99 33) Phenanthrene 25.04 178 524157 3.57 ug/1 99 34) Anthracene 25.17 178 489172 3.35 ug/1 100 35) Di-n-butylphthalate 26.98 149 711742 3.65 ug/1 99 36) Fluoranthene 28.65 202 499302 3.53 ug/1 97 3 9) Pyrene 29.31 202 520971 3.34 ug/1 98 40) Butylbenzylphthalate 31.49 149 242956 2.98 ug/1 94 41) Benzo(a)anthracene 32.96 228 373124 3.46 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.29 149 464037 4.21 ug/1 98 43) Chrysene 33.08 228 396514 3.75 ug/1 99 45) Di-n-Octylphthalate 35.03 149 441606 2.44 ug/1 # 94 46) Benzo(b)fluoranthene 36.03 252 325079 3.18 ug/1 99 47) Benzo(k)fluoranthene 36.09 252 349662 3.33 ug/1 97 48) Benzo(a)pyrene 36.92 252 257289 2.89 ug/1 98 49) Indeno(1,2,3-cd)pyrene 40.77 276 299009 3.36 ug/1 99 50) Dibenz(a,h)anthracene 40.83 278 252322 3.62 ug/1 99 51) Benzo (g,h, Dperylene 41.85 276 276111 3.63 ug/1 95

(#) = qualifier out of range (m) = manual integration REFA.D GCMS1126.M Fri Dec 07 15:45:54 2001 Page 2

NYC-WTC_000035442

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