Document containing calculated reference values for various organic compounds analyzed by GCMS.
NYC-WTC_000035678–000035682Folder label: “GCMS X 11/28/01 A 12/7/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\1\DATA\DECO6O1\REFB .D Vial: 36 Acq On 7 Dec 2001 9:50 am Operator: 209 GALOS Sample 11/28 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 7 15:46 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Compound R.T. Qlon Response Cone Unit Qvalue
30) N-Nitrosodiphenylamine 22.59 168 170007 3.07 ug/1 98 31) 4-Bromophenyl-phenylether 23.65 248 101880 3.32 ug/1 94 32) Hexachlorobenzene 24.07 284 113499 3.36 ug/1 95 33) Phenanthrene 25.04 178 595169 3.60 ug/1 99 3 4) Anthracene 25.17 178 544841 3.31 ug/1 99 35) Di-n-butylphthalate 26.98 149 798918 3.63 ug/1 99 3 6) Fluoranthene 28.65 202 572891 3.59 ug/1 97 3 9) Pyrene 29.31 202 597680 3.30 ug/1 98 40) Butylbenzylphthalate 31.49 149 255862 2.71 ug/1 90 41) Benzo(a)anthracene 32.96 228 426528 3.41 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.29 149 343827 2.69 ug/1 100 43) Chrysene 33.09 228 455991 3.72 ug/1 98 45) Di-n-Octylphthalate 35.03 149 390228 1.93 ug/1 # 96 46) Benzo(b)fluoranthene 36.03 252 355963 3.11 ug/1 99 47) Benzo(k)fluoranthene 36.10 252 386960 3.29 ug/1 98 4 8) Benzo(a)pyrene 36.92 252 274728 2.76 ug/1 98 49) Indeno(1,2,3-cd)pyrene 40.77 276 292356 2.94 ug/1 97 50) Dibenz(a,h)anthracene 40.83 278 242500 3.11 ug/1 96 51) Benzo(g,h,i)perylene 41.85 276 268043 3.15 ug/1 95
(#) = qualifier out of range (m) = manual integration REFB.D GCMS1126.M Fri Dec 07 15:47:46 2001 Page 2
NYC-WTC_000035681
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NYC-WTC_000037239
Reference standard analysis report for gas chromatography-mass spectrometry of sample AD29932 conducted on December 18, 2001.
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GCMS reference standard analysis for sample AD28903 dated December 7, 2001, showing measured concentrations.
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Reference sheet listing expected values and detection limits for volatile organic compounds in WTC samples.
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Laboratory report detailing GCMS calibration analysis for various organic compounds including nitrosamines and chlorobenzenes conducted on December 13, 2001.
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Gas chromatography-mass spectrometry reference report listing concentrations of volatile organic compounds for sample AD28593.
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Calibration data for GCMS analysis of volatile organic compounds dated December 6, 2001.
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Laboratory report of GCMS reference standard analysis for sample AD29665 conducted on December 15, 2001.
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Document containing reference values and recovery data for organic compounds analyzed by GCMS.
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Reference analysis report for DEP sample AE02966 showing measured values for target compounds against detection limits.
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Laboratory report listing recovery percentages for thirteen volatile organic compounds in reference standard AE00109 analyzed on February 14, 2002.
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Reference analysis results for volatile organic compounds analyzed by GCMS on February 8, 2002.
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Reference analysis report for gas chromatography-mass spectrometry quantification of volatile organic compounds conducted on December 29, 2001.
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NYC-WTC_000034949
Form detailing Method 508 parameters and sample volume information for environmental testing procedures.
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Document containing reference values and recovery data for organic compounds analyzed by GCMS.
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GCMS reference standard analysis for sample AD28903 dated December 7, 2001, showing measured concentrations.
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Calibration report detailing response factors for standard compounds used in GCMS analysis of sample AD29135.
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Reference standard analysis report for GCMS testing showing concentrations of target analytes and detection limits.
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Calibration data for GCMS analysis of volatile organic compounds dated December 6, 2001.
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NYC-WTC_000035662
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
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NYC-WTC_000035663
Fragmented document containing method 508 data and sample IDs processed by GCMS in late 2001.
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NYC-WTC_000035664
Laboratory data sheet recording GCMS Method 508 analysis of a blank sample for nitrosamines and chlorinated compounds.
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NYC-WTC_000035674
Calibration data sheet verifying instrument response for nitrosamines and benzene derivatives.
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NYC-WTC_000035683
Laboratory notes stating the GCMS scan of sample AD28898 revealed no unusual compounds.
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