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Laboratory method documentation for sample analysis, Jan 2001

Machine-extracted title · confidence 100%

Form detailing Method 508 parameters and sample volume information for environmental testing procedures.

NYC-WTC_000034949–000034953

Folder label: “GCMS X 11/24/01 A 12/4/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data'File C:\HPCHEM\1\DATA\DEC0 601\REF.D Vial: 10 Acq On 6 Dec 2001 4:15 pm Operator: 209 GALOS Sample 11/24 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 7 15:43 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.59 168 196377 3.49 ug/1 95 31) 4-Bromophenyl-phenylether 23.66 248 122665 3.94 ug/1 98 32) Hexachlorobenzene 24.08 284 128152 3.74 ug/1 96 33) Phenanthrene 25.04 178 687670 4.10 ug/1 99 34) Anthracene 25.17 178 659416 3.95 ug/1 100 35) Di-n-butylphthalate 26.99 149 929012 4.17 ug/1 99 36) Fluoranthene 28.65 202 689551 4.26 ug/1 97 3 9) Pyrene 29.32 202 715253 3.67 ug/1 99 40) Butylbenzylphthalate 31.50 149 344761 3.39 ug/1 95 41) Benzo(a)anthracene 32.96 228 560628 4.17 ug/1 100 42) Bis(2-ethylhexyl)phthalate 33.29 149 514663 3.74 ug/1 99 43) Chrysene 33.09 228 574798 4.35 ug/1 98 45) Di-n-Octylphthalate 35.03 149 676024 2.83 ug/1 # 93 46) Benzo(b)fluoranthene 36.03 252 487830 3.61 ug/1 99 47) Benzo(k)fluoranthene 36.10 252 537559 3.87 ug/1 99 48) Benzo(a)pyrene 36.92 252 392408 3.34 ug/1 99 49) Indeno(1,2,3-cd)pyrene 40.77 276 467584 3.98 ug/1 99 50) Dibenz(a,h)anthracene 40.83 278 387951 4.21 ug/1 96 51) Benzo (g,h,i)perylene 41.86 276 420499 4.18 ug/1 94

(#) = qualifier out of range (m) = manual integration REF.D GCMS1126.M Fri Dec 07 15:44:24 2001 Page 2

NYC-WTC_000034952

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NYC-WTC_000034952Source: NYC Law Department, mirrored locally

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