Calibration data for volatile organic compounds including nitrosamines and chlorinated solvents from December 2001.
NYC-WTC_000036205–000036209Folder label: “GCMS X 12/4/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\DEC1001\REFB.D Vial: 14 Acq On : 10 Dec 2001 11:25 pm Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 14 14:40 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Compound R.T. Qlon Response Cone Unit Qvalue
30) N-Nitrosodiphenylamine 22.59 168 161568 3.77 ug/1 # 92 31) 4-Bromophenyl-phenylether 23.66 248 95192 4.01 ug/1 99 3 2) Hexachiorobenzene 24.07 284 108186 4.14 ug/1 99 3 3) Phenanthrene 25.04 178 532808 4.17 ug/1 99 34) Anthracene 25.17 178 491609 3.86 ug/1 100 35) Di-n-butylphthalate 26.98 149 712643 4.19 ug/1 99 36) Fluoranthene 28.65 202 503193 4.08 ug/1 97 3 9) Pyrene 29.32 202 522689 3.36 ug/1 100 40) Butylbenzylphthalate 31.49 149 234258 3.31 ug/1 # 87 41) Benzo(a)anthracene 32.96 228 380256 4.06 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.29 149 407587 4.26 ug/1 100 43) Chrysene 33.07 228 394091 4.29 ug/1 100 45) Di-n-Octylphthalate 35.03 149 386183 2.64 ug/1 # 93 46) Benzo(b)fluoranthene 36.03 252 331374 4.00 ug/1 98 47) Benzo(k)fluoranthene 36.10 252 382230 4.50 ug/1 99 48) Benzo(a)pyrene 36.92 252 246070 3.42 ug/1 98 49) Indeno(l,2,3-cd)pyrene 40.77 276 257477 3.58 ug/1 95 50) Dibenz(a,h)anthracene 40.83 278 214265 3.80 ug/1 99 51) Benzo(g,h,i)perylene 41.86 276 227563 3.70 ug/1 94
(#) = qualifier out of range (m) = manual integration REFB.D GCMS1126.M Wed Dec 19 16:31:06 2001 Page 2
NYC-WTC_000036208
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NYC-WTC_000036345
Reference standard analysis report for GCMS testing showing concentrations of target analytes and detection limits.
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Form detailing Method 508 parameters and sample volume information for environmental testing procedures.
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Calibration report detailing response factors for standard compounds used in GCMS analysis of sample AD29135.
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Document containing reference values and recovery data for organic compounds analyzed by GCMS.
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Document containing reference values and recovery data for organic compounds analyzed by GCMS.
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Calibration data for GCMS analysis of volatile organic compounds dated December 6, 2001.
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Document containing calculated reference values for various organic compounds analyzed by GCMS.
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GCMS reference standard analysis for sample AD28903 dated December 7, 2001, showing measured concentrations.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037239
Reference standard analysis report for gas chromatography-mass spectrometry of sample AD29932 conducted on December 18, 2001.
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Laboratory report detailing GCMS calibration analysis for various organic compounds including nitrosamines and chlorobenzenes conducted on December 13, 2001.
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Reference analysis report showing measured concentrations of volatile organic compounds in sample AD31662 on February 13, 2002.
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Reference data report for GCMS analysis of sample AE01463 conducted on February 27, 2002.
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NYC-WTC_000036199
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
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NYC-WTC_000036200
Laboratory methodology table documenting sample extraction parameters, surrogate recovery rates, and quality control data for mass spectrometry analysis.
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Laboratory record documenting the extraction method parameters for sample AD29229 analyzed in December 2001.
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NYC-WTC_000036210
Reference analysis results for target analytes used to verify GCMS instrument performance in December 2001.
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NYC-WTC_000036220
Blank sample results showing non-detect levels for target compounds during December 2001 laboratory testing.
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