GCMS reference calculation results, Dec 13 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC0601\REFB.D Vial: 36 Acq On : 7 Dec 2001 9:50 am Operator: 209 GALOS Sample : 11/28 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 7 15:46 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 11.67 152 1123933 20.00 ug/1 -0.03 10) Naphthalene-d8 15.28 136 4274069 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.56 164 2101845 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.98 188 3120542 20.00 ug/1 -0.01 38) Chrysene-dl2 33.01 240 2097503 20.00 ug/1 -0.02 44) Perylene-dl2 37.11 264 1522095 20.00 ug/1 -0.01

System Monitoring Compounds 37) 2,4-DDD 30.06 235 177655 4.78 ug/mL -0.01 Spiked Amount 5.000 Recovery = 95.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.40 74 104885 2.12 ug/1 89 3) bis(2-Chloroethyl)ether 11.10 93 251735 3.24 ug/1 97 4) 1,3-Dichlorobenzene 11.58 146 174584 2.14 ug/1 97 5) 1,4-Dichlorobenzene 11.72 146 194112 2.35 ug/1 99 6) 1,2-Dichlorobenzene 12.23 146 193498 2.54 ug/1 98 7) 2,2' -oxybis (1-Chloropropan 12.57 45 367935 3.72 ug/1 # 93 8) N-Nitroso-di-n-propylamine 12.95 70 151994 3.44 ug/1 94 9) Hexachloroethane 13.06 117 46707 1.55 ug/1 98 11) Nitrobenzene 13.35 77 214532 3.22 ug/1 97 12) 1sophorone 14.00 82 470978 3.67 ug/1 98 13) bis(2-Chloroethoxy)methane 14.69 93 297304 3.45 ug/1 98 14) 1,2,4-Trichlorobenzene 15.17 180 159978 2.58 ug/1 99 15) Naphthalene 15.33 128 657199 3.22 ug/1 100 16) Hexachiorobutadiene 15.88 225 41605 1.38 ug/1 97 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 18.82 162 369654 3.08 ug/1 99 20) Dimethylphthalate 19.93 163 485083 3.47 ug/1 99 21) 2,6-Dinitrotoluene 20.14 165 84879 2.57 ug/1 # 66 2 2) Acenaphthylene 20.09 152 566103 3.36 ug/1 99 23) Acenaphthene 20.65 153 406588 3.37 ug/1 100 24) 2,4-Dinitrotoluene 21.31 165 97062 2.31 ug/1 # 87 25) Diethylphthalate 22.06 149 481447 3.72 ug/1 98 26) 4-Chlorophenyl-phenylether 22.20 204 202516 3.59 ug/1 98 27) Fluorene 22.16 166 440961 3.57 ug/1 98 2 8) Azobenzen/ 1,2-Diphenylhyd 22.66 77 472106 3.53 ug/L 95

(#) = qualifier out of range (m) = manual integration REFB.D GCMS1126.M Fri Dec 07 15:47:43 2001 Page 1

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