GCMS reference standard results Dec 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC1201\REFE.D Vial: 16 Acq On : 12 Dec 2001 5:37 pm Operator: 209 GALOS Sample : gc/ms scan 12/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 12 18:26 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.67 152 934969 20.00 ug/1 -0.03 10) Naphthalene-d8 15.28 136 3648816 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.56 164 1823188 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.97 188 2631849 20.00 ug/1 -0.02 38) Chrysene-dl2 33.01 240 1709568 20.00 ug/1 -0.02 44) Perylene-dl2 37.10 264 1201060 20.00 ug/1 -0.02

System Monitoring Compounds 37) 2,4-DDD 30.05 235 115293 3.68 ug/mL -0.02 Spiked Amount 5.000 Recovery = 73.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.41 74 75601 1.84 ug/1 92 3) bis(2-Chloroethyl)ether 11.10 93 176607 2.74 ug/1 95 4) 1,3-Dichlorobenzene 11.58 146 119433 1.76 ug/1 97 5) 1,4-Dichlorobenzene 11.58 146 119433 1.74 ug/1 98 6) 1,2-Dichlorobenzene 12.23 146 133554 2.11 ug/1 98 7) 2,2'-oxybis(1-Chioropropan 12.57 45 277483 3.38 ug/1 # 91 8) N-Nitroso-di-n-propylamine 12.95 70 117590 3.20 ug/1 95 9) Hexachloroethane 13.06 117 31510 1.26 ug/1 97 11) Nitrobenzene 13.35 77 149235 2.62 ug/1 92 12) 1sophorone 14.00 82 .335235 3.06 ug/1 96 13) bis(2-Chloroethoxy)methane 14.69 93 212102 2.88 ug/1 99 14) 1,2,4-Trichlorobenzene 15.17 180 108870 2.05 ug/1 97 15) Naphthalene 15.33 128 472996 2.71 ug/1 100 16) Hexachlorobutadiene 15.88 225 28497 1.10 ug/1 98 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 18.82 162 258405 2.48 ug/1 98 20) Dimethylphthalate 19.93 163 364216 3.01 ug/1 100 21) 2,6-Dinitrotoluene 20.14 165 58279 2.04 ug/1 # 63 2 2) Acenaphthylene 20.09 152 405363 2.77 ug/1 100 2 3) Acenaphthene 20.64 153 303647 2.91 ug/1 100 24) 2,4-Dinitrotoluene 21.32 165 69848 1.92 ug/1 # 87 25) Diethylphthalate 22.06 149 358886 3.20 ug/1 99 26) 4-Chlorophenyl-phenylether 22.20 204 143422 2.93 ug/1 97 27) Fluorene 22.16 166 321104 2.99 ug/1 97 28) Azobenzen/ 1,2-Diphenylhyd 22.66 77 352017 3.04 ug/L 96

(#) = qualifier out of range (m) = manual integration REFE.D GCMS1126.M Fri Dec 21 12:40:57 2001 Page 1

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