GCMS reference analysis results, sample AD28903, Dec 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DECO7O1\REF. D Vial: 8 Acq On 7 Dec 2001 9:46 pm Operator: 209 GALOS Sample 11/29 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 7 22:34 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.68 152 962412 20.00 ug/1 -0.02 10) Naphthalene-d8 15.27 136 3688185 20.00 ug/1 -0.03 17) Acenaphthene-dl0 20.55 164 1858608 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.98 188 2757222 20.00 ug/1 -0.01 38) Chrysene-dl2 33.01 240 1799956 20.00 ug/1 -0.02 44) Perylene-dl2 37.11 264 1290308 20.00 ug/1 -0.01

System Monitoring Compounds 37) 2,4-DDD 30.05 235 199153 6.07 ug/mL -0.02 Spiked Amount 5.000 Recovery = 121.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.40 74 123121 2.91 ug/1 96 3) bis(2-Chloroethyl)ether 11.10 93 264510 3.98 ug/1 97 4) 1,3-Di chlorobenzene 11.57 146 205671 2.94 ug/1 98 5) 1,4-Dichiorobenzene 11.57 146 205671 2.91 ug/1 99 6) 1,2-Dichlorobenzene 12.23 146 219047 3.36 ug/1 97 7) 2,2’-oxybi s(1-Chloropropan 12.57 45 399037 4.72 ug/1 # 92 8) N-Nitroso-di-n-propylamine 12.95 70 176492 4.66 ug/1 98 9) Hexachloroethane 13.06 117 61616 2.39 ug/1 96 11) Nitrobenzene 13.35 77 228395 3.97 ug/1 93 12) 1sophorone 14.00 82 496421 4.48 ug/1 98 13) bis(2-Chloroethoxy)methane 14.69 93 319390 4.29 ug/1 99 14) 1,2,4-Trichlorobenzene 15.17 180 180856 3.38 ug/1 99 15) Naphthalene 15.33 128 709751 4.03 ug/1 99 16) Hexachiorobutadiene 15.88 225 58934 2.26 ug/1 99 18) Hexachlorocyclopentadiene 18.07 237 617 N.D. 19) 2-Chloronaphthalene 18.82 162 400709 3.78 ug/1 97 20) Dimethylphthalate 19.93 163 524375 4.25 ug/1 100 21) 2,6-Dinitrotoluene 20.14 165 96204 3.30 ug/1 # 63 22) Acenaphthylene 20.08 152 610402 4.10 ug/1 99 2 3) Acenaphthene 20.64 153 442321 4.15 ug/1 98 24) 2,4-Dinitrotoluene 21.31 165 117299 3.16 ug/1 # 88 25) Diethylphthalate 22.06 149 518255 4.53 ug/1 99 26) 4-Chlorophenyl-phenylether 22.20 204 217971 4.37 ug/1 100 27) Fluorene 22.16 166 473760 4.33 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 22.66 77 522974 4.43 ug/L 94

(#) = qualifier out of range (m) = manual integration REF.D GCMS1126.M Wed Dec 12 14:55:32 2001 Page 1

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