GCMS reference results for sample AD29022, Dec 14 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC1001\REF.D Vial: 4 Acq On : 10 Dec 2001 12:40 pm Operator: 209 GALOS Sample : gc/ms scan 11/30 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 10 13:29 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 11.68 152 813906 20.00 ug/1 -0.02 10) Naphthalene-d8 15.27 136 3098214 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.55 164 1566226 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.98 188 2238747 20.00 ug/1 -0.01 38) Chrysene-dl2 33.01 240 1393383 20.00 ug/1 -0.02 44) Perylene-dl2 37.10 264 971828 20.00 ug/1 -0.02

System Monitoring Compounds 37) 2,4-DDD 30.06 235 142893 5.36 ug/mL -0.01 Spiked Amount 5.000 Recovery = 107.20%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.41 74 60901 1.70 ug/1 87 3) bis(2-Chloroethyl)ether 11.10 93 190760 3.40 ug/1 94 4) 1,3-Dichlorobenzene 11.58 146 111733 1.89 ug/1 98 5) 1,4-Dichlorobenzene 11.58 146 111733 1.87 ug/1 99 6) 1,2-Dichlorobenzene 12.23 146 123930 2.25 ug/1 97 7) 2,2’-oxybi s(1-Chioropropan 12.57 45 291304 4.07 ug/1 # 92 8) N-Nitroso-di-n-propylamine 12.95 70 127058 3.97 ug/1 95 9) Hexachloroethane 13.06 117 • 30289 1.39 ug/1 99 11) Nitrobenzene 13.35 77 168616 3.49 ug/1 92 12) Isophorone 14.00 82 363886 3.91 ug/1 97 13) bis(2-Chloroethoxy)methane 14.69 93 228788 3.66 ug/1 98 14) 1,2,4-Trichlorobenzene 15.17 180 107267 2.38 ug/1 100 15) Naphthalene 15.33 128 473058 3.20 ug/1 100 16) Hexachlorobutadiene 15.88 225 33321 1.52 ug/1 98 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 18.83 162 270813 3.03 ug/1 98 20) Dimethylphthalate 19.93 163 394760 3.79 ug/1 99 21) 2,6-Dinitrotoluene 20.14 165 69360 2.82 ug/1 # 63 22) Acenaphthylene 20.09 152 424446 3.38 ug/1 98 2 3) Acenaphthene 20.65 153 309736 3.45 ug/1 99 24) 2,4-Dinitrotoluene 21.32 165 82356 2.63 ug/1 # 86 25) Diethylphthalate 22.06 149 393253 4.08 ug/1 97 26) 4-Chlorophenyl-phenylether 22.20 204 157023 3.73 ug/1 99 2 7) Fluorene 22.16 166 342121 3.71 ug/1 100 28) Azobenzen/ 1,2-Diphenylhyd 22.66 77 383639 3.85 ug/L 92

(#) = qualifier out of range (m) = manual integration REF.D GCMS1126.M Wed Dec 12 15:23:24 2001 Page 1

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