GCMS calibration results, sample AD29135, Dec 2001

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Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC1001\REFB.D Vial: 14 Acq On : 10 Dec 2001 11:25 pm Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 14 14:40 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.68 152 860697 20.00 ug/1 -0.02 10) Naphthalene-d8 15.27 136 3315881 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.55 164 1662948 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.98 188 2413391 20.00 ug/1 -0.01 38) Chrysene-dl2 33.01 240 1570754 20.00 ug/1 -0.02 44) Perylene-dl2 37.10 264 1100836 20.00 ug/1 -0.02

System Monitoring Compounds 37) 2,4-DDD 30.05 235 158704 5.52 ug/mL -0.02 Spiked Amount 5.000 Recovery = 110.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.41 74 94895 2.51 ug/1 91 3) bis(2-Chloroethyl)ether 11.10 93 220924 3.72 ug/1 95 4) 1,3-Dichlorobenzene 11.57 146 164780 2.63 ug/1 98 5) 1,4-Dichlorobenzene 11.57 146 164780 2.60 ug/1 99 6) 1,2-Dichlorobenzene 12.23 146 174414 2.99 ug/1 99 7) 2,2'-oxybis(1-Chioropropan 12.57 45 335238 4.43 ug/1 # 91 8) N-Nitroso-di-n-propylamine 12.95 70 145709 4.30 ug/1 96 9) Hexachloroethane 13.06 117 49286 2.14 ug/1 98 11) Nitrobenzene 13.35 77 186697 3.61 ug/1 92 12) 1sophorone 14.00 82 404324 4.06 ug/1 95 13) bis(2-Chloroethoxy)methane 14.69 93 262078 3.92 ug/1 100 14) 1,2,4-Trichlorobenzene 15.16 180 147729 3.07 ug/1 99 15) Naphthalene 15.33 128 589572 3.72 ug/1 100 16) Hexachlorobutadiene 15.88 225 51711 2.20 ug/1 94 18) Hexachlorocyclopentadiene 18.07 237 682 N.D. 19) 2-Chloronaphthalene 18.83 162 336476 3.55 ug/1 99 20) Dimethylphthalate 19.93 163 437240 3.96 ug/1 99 21) 2,6-Dinitrotoluene 20.14 165 72286m 2.77 ug/1 22) Acenaphthylene 20.08 152 507324 3.81 ug/1 99 2 3) Acenaphthene 20.64 153 369515 3.88 ug/1 99 24) 2,4-Dinitrotoluene 21.31 165 86771 2.61 ug/1 # 91 25) Diethylphthalate 22.06 149 426478 4.17 ug/1 97 26) 4-Chlorophenyl-phenylether 22.20 204 181019 4.05 ug/1 98 27) Fluorene 22.16 166 390540 3.99 ug/1 98 28) Azobenzen/ 1,2-Diphenylhyd 22.66 77 437348 4.14 ug/L 94

(#) = qualifier out of range (m) = manual integration REFB.D GCMS1126.M Fri Dec 14 14:41:43 2001 Page 1

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