GCMS reference results for sample AD29024, Dec 18 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\DEC1001\REFA.D ■ Vial: 26 Acq On : 11 Dec 2001 1:04 pm Operator: 209 GALOS Sample : gc/ms scan ll/30a Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 11 13:52 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.67 152 1064763 20.00 ug/1 -0.02 10) Naphthalene-d8 15.28 136 4031867 20.00’ ug/1 -0.02 17) Acenaphthene-dlO 20.55 164 2071230 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.98 188 3045607 20.00 ug/1 -0.02 38) Chrysene-dl2 33.01 240 1987513 20.00 ug/1 -0.02 44) Perylene-dl2 37.10 264 1395798 20.00 ug/1 -0.02

System Monitoring Compounds 37) 2,4-DDD 30.05 235 169097 4.66 ug/mL -0.02 Spiked Amount 5.000 Recovery = 93.20%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.42 74 92401 1.97 ug/1 88 3) bis(2-Chloroethyl)ether 11.10 93 228840 3.11 ug/1 94 4) 1,3-Dichlorobenzene 11.57 146 151468 1.96 ug/1 98 5) 1,4-Dichlorobenzene 11.57 146 151468 1.93 ug/1 99 6) 1,2-Diehlorobenzene 12.23 146 167251 2.32 ug/1 100 7) 2,2*-oxybis(1-Chloropropan 12.56 45 340066 3.63 ug/1 # 92 8) N-Nitroso-di-n-propylamine 12.96 70 149729 3.58 ug/1 97 9) Hexachloroethane 13.06 117 41544 1.46 ug/1 93 11) Nitrobenzene 13.35 77 192855 3.07 ug/1 95 12) Isophorone 14.00 82 428568 3.54 ug/1 96 13) bis(2-Chloroethoxy)methane 14.69 93 269526 3.31 ug/1 98 14) 1,2,4-Trichlorobenzene 15.17 180 141155 2.41 ug/1 97 15) Naphthalene 15.34 128 575242 2.99 ug/1 99 16) Hexachlorobutadiene 15.89 225 36655 1.28 ug/1 96 18) Hexachlorocyclopentadiene 18.07 237 295 N.D. 19) 2-Chloronaphthalene 18.83 162 333215 2.82 ug/1 98 20) Dimethylphthalate 19.94 163 474298 3.45 ug/1 99 21) 2,6-Dinitrotoluene 20.15 165 84257 2.59 ug/1 # 66 22) Acenaphthylene 20.08 152 512565 3.09 ug/1 99 23) Acenaphthene 20.64 153 370093 3.12 ug/1 99 24) 2,4-Dinitrotoluene 21.31 165 102192 2.47 ug/1 # 90 25) Diethylphthalate 22.06 149 469668 3.69 ug/1 98 26) 4-Chlorophenyl-phenylether 22.19 204 184589 3.32 ug/1 100 27) Fluorene 22.16 166 406792 3.34 ug/1 97 28) Azobenzen/ 1,2-Diphenylhyd 22.66 77 461142 3.50 ug/L 97

(#) = qualifier out of range (m) = manual integration REFA.D GCMS1126.M Wed Dec 12 15:25:25 2001 Page 1

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