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GCMS calibration results for sample AD29932, Dec 2001

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Calibration data report for gas chromatography-mass spectrometry instruments used to analyze sample AD29932 on December 18, 2001.

NYC-WTC_000037235–000037238

Folder label: “GCMS X 12/11/01 A 12/18/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC18O1\CAL25.D Vial: 2 Acq On 18 Dec 2001 5:02 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 15 9:51 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : NPO91101

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.61 168 1247693 25.52 ug/1 # 90 31) 4-Bromophenyl-phenylether 23.67 248 684960 25.29 ug/1 99 3 2) Hexachlorobenzene 24.09 284 783429 26.30 ug/1 99 3 3) Phenanthrene 25.05 178 3654063 25.06 ug/1 99 3 4) Anthracene 25.19 178 3682077 25.33 ug/1 99 35) Di-n-butylphthalate 27.00 149 4902660 25.27 ug/1 99 36) Fluoranthene 28.67 202 3659088 26.00 ug/1 98 3 9) Pyrene 29.33 202 3731126 22.40 ug/1 98 40) Butylbenzylphthalate 31.51 149 1924024 22.12 ug/1 90 41) Benzo(a)anthracene 32.97 228 2815657 24.49 ug/1 100 42) Bis(2-ethylhexyl)phthalate 33.30 149 2534876 21.57 ug/1 98 43) Chrysene 33.10 228 2730673 24.22 ug/1 99 45) Di-n-Octylphthalate 35.04 149 4036354 20.60 ug/1 # 93 46) Benzo(b)fluoranthene 36.06 252 2812742 25.36 ug/1 99 47) Benzo(k)fluoranthene 36.12 252 2782360 24.44 ug/1 99 48) Benzo(a)pyrene 36.95 252 2382959 24.71 ug/1 99 49) Indeno(1,2,3-cd)pyrene 40.81 276 2375150 24.63 ug/1 96 50) Dibenz(a,h)anthracene 40.88 278 1872524 24.80 ug/1 96 51) Benzo(g,h,i)perylene 41.92 276 1962627 23.82 ug/1 93

(#) = qualifier out of range (m) = manual integration CAL25.D GCMS1126.M Tue Jan.15 09:51:51 2002 Page 2

NYC-WTC_000037237

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NYC-WTC_000037237Source: NYC Law Department, mirrored locally

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