GCMS calibration report, December 2001

NYC 9/11 Public Portal Document oe Quantitation Report (QT Reviewed) G Data File : C:\HPCHEM\1\DATA\DEC1901\CAL25A.D Vial: 2 Acq On : 20 Dec 2001 10:13 am Operator: 209 GALOS Sample : Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 2 10:02 2002 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator] Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : NPO91101 Internal Standards R.T. Qlon Response Conc Units Dev (Min 1) 1,4-Dichlorobenzene-d4 11.68 152 1657958 20.00 ug/l -0.02 10) Naphthalene-ds 15.29 136 6471592 20.00 ug/l -0.02 17) Acenaphthene-d10 20.57 164 3205530 20.00 ug/1 0.00 29) Phenanthrene-d10 24.99 188 4922090 20.00 ug/l 0.00 38) Chrysene-d12 33.04 240 3527199 20.00 ug/1 0.00 44) Perylene-d12 37.13 264 2528103 20.00 ug/l 0.01 System Monitoring Compounds 37) 2,4-DDD 0.00 235 od 0.00 ug/ml Spiked Amount 5.000 Recovery = 0.00% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.40 74 2023386m 27.75 ug/l 3) bis(2-Chloroethyl) ether 11.12 93 2993816 26.16 ug/1 95 4) 1,3-Dichlorobenzene 11.58 146 3015663 25.01 ug/l 99 5) 1,4-Dichlorobenzene 11.73 146 3021548 24.78 ug/l 99 6) 1,2-Dichlorobenzene 12.23 146 2755682 24.51 ug/l 98 7) 2,2'-oxybis(1-Chloropropan 12.57 45 4565295 31.32 ug/1 96 8) N-Nitroso-di-n-propylamine 12.99 70 1974198 ~ 30.28 ug/l 95 9) Hexachloroethane 13.06 117 1200316 27.07 ug/l 92 11) Nitrobenzene 13.37 77 2921673 28.97 ug/l 93 12) Isophorone 14.02 82 5519511 28.40 ug/l 95 13) bis(2-Chloroethoxy)methane 14.70 93 3559239 27.26 ug/1 99 14) 1,2,4-Trichlorobenzene 15.18 180 2345009 24.95 ug/1 99 15) Naphthalene 15.35 128 7809535 25.25 ug/l 99 16) Hexachlorobutadiene 15.89 225 1177009 25.70 ug/l 98 18) Hexachlorocyclopentadiene 18.06 237 473619 20.51 ug/l 98 19) 2-Chloronaphthalene 18.83 162 4569264 24.99 ug/1 97 20) Dimethylphthalate 19.96 163 5380975 25.26 ug/1 99 21) 2,6-Dinitrotoluene 20.17 165 1295025m 25.73 ug/l 22) Acenaphthylene 20.09 152 6536245 25.43 ug/l 100 23) Acenaphthene 20.66 153 4616906 25.12 ug/1 100 24) 2,4-Dinitrotoluene 21.34 165 1686909 26.36 ug/l # 88 25) Diethylphthalate 22.10 149 5223736 26.50 ug/l 99 26) 4-Chlorophenyl-phenylether 22.21 204 2205018 25.62 ug/1 99 27) Fluorene 22.19 166 4770143 25.30 ug/l 100 28) Azobenzen/ 1,2-Diphenylhyd 22.68 77° 5754067 28.25 ug/L 93 (#) = qualifier out of range (m) = manual integration CAL25A.D GCMS1126.M Wed Jan 02 10:04:03 2002 Page 1 NYC-WTC_000016808