GCMS analysis summary, sample AD27392, Dec 2001

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Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\JAN1502\27392 . D Vial: 9 Acq On : 15 Jan 2002 6:46 pm Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclohexanecarbonitrile, 1- (1- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

32.58 0.50 ug/1 115307 Chrysene-dl2 32.80

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexanecarbonitrile, l-(l-piper 192 C12H20N2 003867-15-0 30 2 Benzoic acid/ ethyl ester 150 C9H10O2 000093-89-0 27 3 Benzoic acid, 2-methylhydrazide 150 C8H10N2O 001660-24-8 12 4 Phthalicacid, diisooctyl ester 390 C24H3804 001330-91-2 12 Abundance * Scan 2999 (32.578 min): 27392.D (-) m/z 104.95 100.00%

N 105

149 5000 55 77 41 Pw „ Tpr +4lllAu4l.,A4lMJ ,163 BuI————...... m/z->___ 20 30 40 50 60... 70 80 90 100110120130140150160170180190 200 210 32.20 32.40 32.60 32.80 33.00 192 207 m/z 149.0.0 B—BB*—B"t08A8414A8d2*88 60.40% Abundance #20781: Cyclohexanecarbonitrile, 1-(1-piperidinyl)- 149

' I ' ‘ ' I 1 ‘ ' I ' ' '" I ' 1‛d • 5000 32.20 32.40 32.60 32.80 33.00

A 42 at 122 136 164 m/z 55.00 46.75% 84 110 h i ,i 191 . ।।11।।।।।I'... 11.1।।1 .>■ । is, ।.,., ।, 11.., ।.... ।, miz—>__ 20 30 40 50 60-70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance .28 Benzclo at thicoter 105 •MWy TI T T TT 32.20 32.40 32.60 32.80 33.00 5000 77 m/z 77.05 41.69% 51 122 27 150

AN i 37 TITT10m111—T p-rTTpTnnyrTTTpTnTYrrrrpTTTpnnTpTTTpTT-rpvTTyTTTTp-TTT^^ m/z->_ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #9664: Benzoic acid, 2-methylhydrazide aa 4 i • ' ‘ * i • ’ ’r IM 105 32.20 32.40 32.60 32.80 33.00 m/z 41.05 35.82% 77 5000

51 1 | ‘}‘m1B1—1—OE220-83T 121 mm ‘‘11241158171-11111111113079111111328813 _15 m/z->20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 210 ——30—38TT3T ptood . " vyv 32.20 32.40 32.60 32.80 33.00

27392.D GCMS1126.M Mon Feb 04 15:00:50 2002 Page 3

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