GCMS analysis summary, sample AD27392, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\JAN1502\27392.D Vial: 9 Acq On : 15 Jan 2002 6:46 pm Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Ethanol, 2,2,2-trichloro- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

7.59 0.44 ug/1 115813 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethanol, 2,2,2-trichloro- 148 C2H3C130 000115-20-8 9 2 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 9 3 1-Fluorononane 146 C9H19F 000463-18-3 9 4 Heptacosane 380 C27H56 000593-49-7 9 Abundance Scan 277 (7.590 min): 27392.D (-) m/z 4 .95 “ 100.00% 43

5000

127 rTr vi . . . 1 ... 1 1 . . 50 61 74 83 97 7.20 7.40 7.60 7.80 8.00 38 1 1 - r 1 ′ .. i ■ । ■ ■ i1 i' li 117 II m/z 126.9.0 12.94% vnlz~> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #66530: Ethanol, 2,2,2-trichloro- 31

5000 7.20 7.40 7.60 7.80 8.00 49 m/z 124.8,0 12.06% 77। 84 . ■ ■ i1 ■111'11111' “ ' i ■ ■ ’I ■ ■i■•■■i■ ■ ■ ■ i1 11 1 95 TTI 113 121 11 ’ ’ ’ I' ‘ 150 i ■ ‘ * i * ■ ■ i miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #12247:2ropauone 1 43 ■ i ■ ' ‘ ‘ i ■ ■ ‘ 1 i • ■ ■ ■ i ■ ‘ ‘ ■ i ‘ ■ 7.20 7.40 7.60 7.80 8.00 5000 m/ z 82.95 9.91%

15 35 85 97 117 125 1111'111 ■ “ ‘i “ ■•i•‘‘■i■1 “ i••■•I■i■■■■i' “ 11‘‘‘'i‘ ‘ “ i ‘ ‘ ‘ i “ ‘ ‘ I ‘ ‘ i ‘ ‘ m/z-> 10 20_ 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #8922: 1-Fluorononane • i ' • ‘ ■ i ■ • ■ ■ i ' ■ ■ • i ‘ ■ i ■ ‘ 43 7.20 7.40 7.60 7.80 8.00 m/z 96.95 8.68% 5000 56 27 70 84 97

" i “ ■' i ‘ ‘ i " ' • i I 1 ' I ‘1 ■ P • ■ ■ i ■"1111 ■ ■ i ■ ■ ■111 ■ ■11'" 11 ■ ■ ■11 ■ • ......... 1.......... m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 7.20 7.40 7.60 7.80 8.00

27392.D GCMS1126.M Mon Feb 04 15:00:45 2002 Page 2

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