GCMS analysis summary, sample AD27392, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\JAN1502\27392.D Vial: 9 Acq On : 15 Jan 2002 6:46 pm Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.45 3.08 ug/1 814637 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 2 Pentane, 3 -methoxy- 102 C6H140 036839-67-5 9 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 7 4 N-Ethylformamide _____ 73 C3H7NO 000627-45-2 5 Abundance Scan 262 (7.452 min): 27392.D (-) m/z 72.95 100.00% 73

5000 43 • • i ■ ■ ■ ■ i ’4 ‘ i ' ■ 7.20 7.40 7.60 7.80 0— 38 |t J 50,55..61 , 67, j , 87 103 • i • • ■ ■ । । m/z 43.00 32.13% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #845: Silane, tetramethyl- 73

5000 7.20 7.40 7.60 7.80 45 m/z 44.95 11.90% 15 31 55 88 * i » * I’t’l 1 1 ■ ' i 1 ■ • i ■ ■ ■ 1 i ■ ■ ■ ■ I 1 1 1 1 1 1 1 m/z->__ 10 20 30 40 50 60 70 80 90 100 110 Abundance 73 ■ i1 TKBBddnn—mmom 7.20 7.40 7.60 7.80 5000 m/z 41.05 11.56% 45

27 33 39 55 **1*/=*naa*u/A“111/1* mrer 1III11 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #763: 1-Butanamine, 3-methyl- 1/*/*1/d*/——11///11/n/n/f1/maR" 7.20 7.40 7.60 7.80 m/z 71.00 7.04% 5000

miz-> ' ‘ i ■ 10 15 ' i ‘ 1 20 41 55 70 P T-|-i-r-r-r-p-r-r-r-|-r-r 30 40 50 87 1 1 ! ■ ■ *'1 1 1 1 1 1 I ' 1 1 1 I 1 1 60 70 80 90 100 110 = m. 7.20 7.40 7.60 7.80

27392.D GCMS1126.M Mon Feb 04 15:00:40 2002 Page 1

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