GCMS analysis results, sample AD31379, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report 9 Data File : C:\HPCHEM\1\DATA\JANI502\31379.D Vial: 15 Acq On : 16 Jan 2002 12:40 am Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.44 4.87 ug/1 1155090 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, tetramethyl - 88 C4H12Si 000075-76-3 9 2 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 1,3-Di xolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 Abundance Scan 261 (7.441 min): 31379.D (-) m/z 73.00 100.00% 73

5000 43

87 103 7.00 7.20 7.40 7.60 7.80 | 50 55 60 67, । 4 38,4 1 ■ i ■ ■ ■ 1 i • ■ ■ • i ■ • • ■ i ■ ■ m/z 43.05 33.27% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62932: Silane, tetramethyl- 73

5000 7.00 7.20 7.40 7.60 7.80 45 m/z 45.05 11.82% 15 , / 53 59 I 88 1 1 i 1 ■ 1 1 I ‘ 1 1 1 I 1 ' 1 1 1 1 ri 1 I’l’i । ‘ ■ ■ i ■ 1 ■ ■ i ' ■ ■ ■ i • ■ ■ ‘ i ■ ■ ■ • i ■ 1 m/z-> 10__ 20___ 30 _ 40 50 60 70 80 90 100 110 Abundance -783 1 Botana ' 1 30 T—ndmmu—mmTTT 7.00 7.20 7.40 7.60 7.80 5000 m/z 41.03 11.56%

15 41 55 70 87 ■ 1 i ' • ‘ ■ i • ■ ■ ■ i • ■ ■ ■ i 1 1 ■ ‘ i • ’"1 i j i i i i । i i !I111*II*I m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 7.00 7.20 7.40 7.60 7.80 73 m/z 71.0.0 6.77% 5000 44 58 15 m/z-> —r" ■ i ■ ■ l'- ' 10 20 30 —pl 40 ji FTnummmOTumTTT 50 60 70 80 90 100 1///n/d/nmmt11183 110 7.00 7.20 7.40 7.60 7.80

31379.D GCMS1126.M Mon Feb 04 15:09:03 2002 Page 1

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