GCMS calibration table June 3, 2002, DEP Labs

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAY31O2\REF1.D Vial: 4 Acq On : 31 May 2002 2:54 pm Operator: Morgan Sample : gc/ms scan 5/29 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jun 3 9:23 2002 Quant Results File::GCMS0531. RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 31 09:43:55 2002 Response via : Initial Calibration DataAcq Meth : GCMS0531

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) l,4-Dichlorobenzene-d4 12.06 152 508540 40.00 ug/1 -0.02 10) Naphthalene-d8 15.70 136 2041534 40.00 ug/1 -0.02 17) Acenaphthene-diO 20.99 164 986161 40.00 ug/1 0.00 3 0) Phenanthrene-dl0 25.43 188 1557848 40.00 ug/1 0.00 38) Chrysene-dl2 33.48 240 974666 40.00 ug/1 -0.03 44) Perylene-dl2 37.66 264 617967 40.00 ug/1 -0.03 System Monitoring Compounds 28) TCMX 23.13 209 221502 32.46 ug/L -0.02 Spiked Amount 40.000 Recovery 81.15% Target Compounds Qvalue 2) N-nitrosodimethylamine 5.72 74 157590 10.12 ug/1 99 3) bis(2-Chloroethyl)ether 11.47 93 303686 14.93 ug/1 98 4) 1,3-Dichlorobenzene 11.97 146 280763 13.89 ug/1 100 5) 1,4-Dichlorobenzene 12.11 146 295569 13.51 ug/1 100 6) 1,2-Dichlorobenzene 12.62 146 285510 14.82 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 12.95 45 494528 15.56 ug/1 99 8) N-Nitrosodi-n-propylamine 13.34 70 215513 15.33 ug/1 98 9) Hexachloroethane 13.47 117 93540 10.82 ug/1 97 11) Nitrobenzene 13.74 77 289370 15.35 ug/1 99 12) 1sophorone 14.39 82 626919 17.73 ug/1 99 13) bis(2-Chloroethoxy)methane 15.08 93 369853 15.92 ug/1 99 14) 1,2,4-Trichlorobenzene 15.59 180 237612 15.02 ug/1 97 15) Naphthalene 15.75 128 906679 16.88 ug/1 100 16) Hexachlorobutadiene 16.30 225 87809 12.60 ug/1 99 18) Hexachlorocyclopentadiene 18.49 237 24395 4.03 ug/1 99 19) 2-Chloronaphthalene 19.25 162 474661 18.07 ug/1 99 20) Dimethylphthalate 20.35 163 579208 17.35 ug/1 99 21) 2,6-Dinitrotoluene 20.56 165 119794 15.89 ug/1 98 2 2) Acenaphthylene 20.52 152 736495 15.63 ug/1 99 23) Acenaphthene 21.09 153 502793 17.71 ug/1 99 24) 2,4-Dinitrotoluene 21.73 165 151610 17.18 ug/1 99 25) Diethylphthalate 22.48 149 585761 18.94 ug/1 99 26) 4-Chlorophenylphenylether 22.63 204 263647 17.93 ug/1 99 27) Fluorene 22.60 166 548111 19.01 ug/1 99 29) Azobenzene 23.10 77 596786 15.63 ug/L 96 31) N-Nitrosodiphenylamine 23.02 168 206810 18.18 ug/1 97 32) 4-Bromophenylphenylether 24.10 248 134012 17.15 ug/1 95 33) Hexachlorobenzene 24.52 284 155950 18.22 ug/1 97 34) Phenanthrene 25.49 178 793801 18.13 ug/1 99 (#) = qualifier out of range (m) = manual integration REFl.D GCMS0531.M Mon Jun 03 09:24:36 2002 Page 1

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