GCMS reference results for VOCs, sample AE12535, June 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File C:\HPCHEM\l\DATA\JUN0302\REFAl.D Vial: 14 Acq On 3 Jun 2002 10:01 pm Operator: Sample gc/ms scan 5/28 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jun 4 11:35 2002 Quant Results File: GCMS0531.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 31 09:43:55 2002 Response via : Initial Calibration DataAcq Meth : GCMS0531

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) l,4-Dichlorobenzene-d4 12.06 152 499600 40.00 ug/1 -0.01 10) Naphthalene-d8 15.70 136 2013512 40.00 ug/1 -0.01 17) Acenaphthene-diO 21.00 164 972143 40.00 ug/1 0.00 30) Phenanthrene-diO 25.43 188 1518931 40.00 ug/1 0.00 38) Chrysene-dl2 33.48 240 912738 40.00 ug/1 -0.02 44) Perylene-dl2 37.66 264 549572 40.00 ug/1 -0.02 System Monitoring Compounds 28) TCMX 23.14 209 205663 30.58 ug/L -0.01 Spiked Amount 40.000 Recovery 76.45% Target Compounds Qvalue 2) N-nitrosodimethylamine 5.72 74 144557 9.45 ug/1 97 3) bis(2-Chloroethyl)ether 11.47 93 290946 14.56 ug/1 99 4) 1,3-Dichlorobenzene 11.96 146 253810 12.79 ug/1 98 5) 1,4-Dichlorobenzene 12.11 146 268296 12.48 ug/1 100 6) 1,2-Dichlorobenzene 12.62 146 264405 13.97 ug/1 98 7) 2,2’-oxybis(1-Chloropropan 12.96 45 479131 15.35 ug/1 98 8) N-Nitrosodi-n-propylamine 13.33 70 201792 14.61 ug/1 100 9) Hexachloroethane 13.47 117 85561 10.08 ug/1 96 11) Nitrobenzene 13.74 77 267906 14.41 ug/1 99 12) 1sophorone 14.40 82 575773 16.51 ug/1 99 13) bis(2-Chloroethoxy)methane 15.08 93 348858 15.23 ug/1 99 14) 1,2,4-Trichlorobenzene 15.58 180 223393 14.31 ug/1 99 15) Naphthalene 15.76 128 866722 16.36 ug/1 100 16) Hexachlorobutadiene 16.30 225 80820 11.76 ug/1 98 18) Hexachlorocyclopentadiene 18.49 237 14150 2.37 ug/1 95 19) 2-Chloronaphthalene 19.25 162 449926 17.38 ug/1 100 20) Dimethylphthalate 20.35 163 532214 16.17 ug/1 98 21) 2,6-Dinitrotoluene 20.56 165 109644 14.75 ug/1 95 2 2) Acenaphthylene 20.52 152 681814 14.67 ug/1 99 2 3) Acenaphthene 21.08 153 467815 16.72 ug/1 99 24) 2,4-Dinitrotoluene 21.73 165 132610 15.24 ug/1 100 25) Diethylphthalate 22.48 149 539287 17.69 ug/1 100 26) 4-Chlorophenylphenylether 22.63 204 245055 16.90 ug/1 100 27) Fluorene 22.60 166 514457 18.10 ug/1 99 29) Azobenzene 23.09 77 556614 14.78 ug/L 99 31) N-Nitrosodiphenylamine 23.02 168 182867 16.49 ug/1 98 32) 4-Bromophenylphenylether 24.09 248 122797 16.11 ug/1 99 33) Hexachlorobenzene 24.52 284 145797 17.47 ug/1 99 3 4) Phenanthrene 25.50 178 735104 17.22 ug/1 99 (#) = qualifier out of range (m) = manual integration REFAI.D GCMS0531.M Tue Jun 04 11:37:04 2002 Page 1

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