GCMS reference analysis report sample AE12094, June 2002

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAY3102\REFA2.D Vial: 15 Acq On 1 Jun 2002 1:46 am Operator: Morgan Sample gc/ms scan 5/30 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jun 3 11:31 2002 Quant Results File :GCMS0531. RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 31 09:43:55 2002 Response via : Initial Calibration DataAcq Meth : GCMS0531

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) l,4-Dichlorobenzene-d4 12.06 152 514214 40.00 ug/1 -0.01 10) Naphthalene-d8 15.69 136 2081026 40.00 ug/1 -0.02 17) Acenaphthene-diO 21.00 164 996978 40.00 ug/1 0.00 30) Phenanthrene-diO 25.43 188 1580441 40.00 ug/1 0.00 38) Chrysene-dl2 33.48 240 1043006 40.00 ug/1 -0.02 44) Perylene-dl2 37.66 264 679960 40.00 ug/1 -0.02 System Monitoring Compounds 28) TCMX 23.14 209 212543 30.81 ug/L -0.01 Spiked Amount 40.000 Recovery 77.03% Target Compounds Qvalue 2) N-nitrosodimethylamine 5.73 74 147011 9.34 ug/1 98 3) bis(2-Chloroethyl)ether 11.47 93 284139 13.82 ug/1 99 4) 1,3-Dichlorobenzene 11.96 146 253438 12.40 ug/1 100 5) 1,4-Dichlorobenzene 12.11 146 269005 12.16 ug/1 99 6) 1,2-Dichiorobenzene 12.62 146 264560 13.58 ug/1 99 7) 2,2'-oxybi s(1-Chioropropan 12.95 45 470944 14.65 ug/1 99 8) N-Nitrosodi-n-propylamine 13.33 70 205446 14.45 ug/1 99 9) Hexachloroethane 13.47 117 80625 9.23 ug/1 98 11) Nitrobenzene 13.74 77 267968 13.95 ug/1 98 12) 1sophorone 14.40 82 589037 16.34 ug/1 97 13) bis(2-Chloroethoxy)methane 15.08 93 347917 14.69 ug/1 99 14) 1,2,4-Trichiorobenzene 15.58 180 219433 13.60 ug/1 99 15) Naphthalene 15.75 128 855528 15.62 ug/1 100 16) Hexachlorobutadiene 16.30 225 69767 9.82 ug/1 97 18) Hexachlorocyclopentadiene 18.49 237 21778 3.56 ug/1 99 19) 2-Chloronaphthalene 19.25 162 449552 16.93 ug/1 99 20) Dimethylphthalate 20.34 163 555444 16.46 ug/1 98 21) 2,6-Dinitrotoluene 20.56 165 114822 15.06 ug/1 98 22) Acenaphthylene 20.52 152 693791 14.56 ug/1 100 23) Acenaphthene 21.08 153 470674 16.40 ug/1 99 24) 2,4-Dinitrotoluene 21.73 165 145603 16.32 ug/1 97 25) Diethylphthalate 22.48 149 566585 18.13 ug/1 100 26) 4-Chlorophenylphenylether 22.63 204 251596 16.92 ug/1 99 27) Fluorene 22.60 166 522520 17.93 ug/1 98 2 9) Azobenzene 23.09 77 571601 14.80 ug/L 99 31) N-Nitrosodiphenylamine 23.02 168 206684 17.91 ug/1 97 32) 4-Bromophenylphenylether 24.09 248 128766 16.24 ug/1 96 3 3) Hexachiorobenzene 24.52 284 149427 17.21 ug/1 99 3 4) Phenanthrene 25.49 178 761999 17.15 ug/1 100 (#) = qualifier out of range (m) = manual integration REFA2.D GCMS0531.M Mon Jun 03 11:33:28 2002 Page 1

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