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GCMS calibration table June 3, 2002, DEP Labs

Machine-extracted title · confidence 95%

Calibration data table for GCMS analysis containing internal standards and surrogate compounds dated June 3, 2002.

NYC-WTC_000014875–000014882

Folder label: “GCMS X 5/29/02 A 5/31/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAY31O2\REF1.D Vial: 4 Acq On : 31 May 2002 2:54 pm Operator: Morgan Sample : gc/ms scan 5/29 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jun 3 9:23 2002 Quant Results File: GCMS0531 .RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 31 09:43:55 2002 Response via : Initial Calibration DataAcq Meth : GCMS0531

Compound R.T. Qlon Response Cone Unit Qvalue

35) Anthracene 25.62 178 739407 16.18 ug/1 100 36) Di-n-butylphthalate 27.41 149 1013286 18.05 ug/1 100 3 7) Fluoranthene 29.11 202 811486 17.44 ug/1 100 3 9) Pyrene 29.79 202 843710 19.29 ug/1 97 40) Butylbenzylphthalate 31.93 149 378070 16.89 ug/1 100 41) Benzo(a)anthracene 33.42 228 554225 17.27 ug/1 . 99 42) Bis(2-ethylhexyl)phthalate 33.71 149 500527 17.02 ug/1 98 43) Chrysene 33.55 228 584317 18.36 ug/1 99 45) Di-n-Octylphthalate 35.45 149 673523 14.99 ug/1 # 98 4 6) Benzo(b)fluoranthene 36.51 252 , 439114 16.84 ug/1 99 4 7) Benzo(k)fluoranthene 36.57 252 481820 17.82 ug/1 99 48) Benzo(a)pyrene 37.46 252 322208 12.79 ug/1 98 49) Indeno(l,2,3-cd)pyrene 41.62 276 345618 14.64 ug/1 99 50) Dibenz(a,h)anthracene 41.70 278 300373 16.17 ug/1 99 51) Benzo(g,h,i)perylene 42.81 276 304467 15.81 ug/1 99

(#) = qualifier out of range (m) = manual integration REFl.D GCMS0531.M Mon Jun 03 09:24:37 2002 Page 2

NYC-WTC_0000 14876

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NYC-WTC_000014876Source: NYC Law Department, mirrored locally

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