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GCMS reference data sample AE12152, May 2002

Machine-extracted title · confidence 90%

Reference analysis report for GCMS testing of sample AE12152 listing organic compounds and response values.

NYC-WTC_000013325–000013332

Folder label: “GCMS X 5/22/02 A 5/25/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAY2402\REF1.D Vial: 4 Acq On : 24 May 2002 6:29 pm Operator: Morgan Sample : gc/ms scan 5/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 28 11:42 2002 Quant Results File; GCMS0520. RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue May 28 11:39:13 2002 Response via : Initial Calibration DataAcq Meth : GCMS0520

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.74 178 652120 15.46 ug/1 99 36) Di-n-butylphthalate 27.52 149 885410 15.86 ug/1 99 37) Fluoranthene 29.22 202 654353 15.77 ug/1 100 39) Pyrene 29.90 202 670782 19.49 ug/1 95 40) Butylbenzylphthalate 32.05 149 288771 16.42 ug/1 90 41) Benzo(a)anthracene 33.55 228 418932 16.31 ug/1 99 42) Bis(2-ethylhexyl)phthalate' 33.83 149 381753 16.51 ug/1 # 97 43) Chrysene 33.68 228 451953 17.82 ug/1 99 45) Di-n-Octylphthalate 35.58 149 487533 12.93 ug/1 # 91 46) Benzo(b)fluoranthene 36.65 252 357983m 14.74 ug/1 47) Benzo(k)fluoranthene 36.72 252 396838m 15.79 ug/1 48) Benzo(a)pyrene 37.63 252 272458 12.08 ug/1 # 95 49) Indeno(l,2,3-cd)pyrene 41.89 276 315541 14.56 ug/1 98 50) Dibenz(a,h)anthracene 41.97 278 273509 15.79 ug/1 95 51) Benzo(g,h,i)perylene 43.11 276 283440 16.36 ug/1 95

(#) = qualifier out of range (m) = manual integration REF1.D GCMS0520.M Tue May 28 11:42:23 2002 Page 2

NYC-WTC_0000 13328

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NYC-WTC_000013328Source: NYC Law Department, mirrored locally

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