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← Document results/DEP Box 15/GCMS X 5/23/02 A 5/29/02
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GCMS calibration report, DEP Box 15, May 2002

Machine-extracted title · confidence 95%

Calibration results for GCMS analysis of volatile organic compounds including nitrosamines and chlorinated benzenes.

NYC-WTC_000013787–000013794

Folder label: “GCMS X 5/23/02 A 5/29/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAY29O2\REF1.D Vial: 4 Acq On : 29 May 2002 2:17 pm Operator: Morgan Sample : gc/ms scan 5/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 30 8:16 2002 Quant Results File :GCMS0528. RES *e- Quant Method : C:\HPCHEM\1\METHODS\GCMS0528.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue May 28 08:55:48 2002 Response via : Initial Calibration DataAcq Meth : GCMS0528

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.62 178 742626 16.68 ug/1 36) Di-n-butylphthalate 27.41 149 1134267 19.26 ug/1 3 7) Fluoranthene 29.11 202 872041 19.92 ug/1 39) Pyrene 29.78 202 899786 22.79 ug/1 40) Butylbenzylphthalate 31.93 149 409754 20.31 ug/1 41) Benzo(a)anthracene 33.42 228 579689m 19.67 ug/1 42) Bis(2-ethylhexyl)phthalate 33.71 149 562397 21.20 ug/1 43) Chrysene 33.55 228 627350 21.55 ug/1 45) Di-n-Octylphthalate 35.45 149 771431 19.24 ug/1 # 91 46) Benzo(b)fluoranthene 36.51 252 501559 19.42 ug/1 99 47) Benzo(k)fluoranthene 36.58 252 483378 18.09 ug/1 99 4 8) Benzo(a)pyrene 37.47 252 310458 12.95 ug/1 97 49) Indeno(1,2,3-cd)pyrene 41.62 276 376868 16.35 ug/1 99 50) Dibenz(a,h)anthracene 41.69 278 325979 17.70 ug/1 98 51) Benzo(g,h,i)perylene 42.80 276 338703 18.39 ug/1 98

(#) = qualifier out of range (m) = manual integration REFl.D GCMS0528.M Thu May 30 08:16:55 2002 Page 2

NYC-WTC_000013793

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NYC-WTC_000013793Source: NYC Law Department, mirrored locally

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