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GCMS calibration data, DEP Labs, May 2002

Machine-extracted title · confidence 100%

Calibration results for gas chromatography mass spectrometry analysis of volatile organic compounds from May 31, 2002.

NYC-WTC_000014746–000014753

Folder label: “GCMS X 5/29/02 A 5/30/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAY3OO2\REF1.D Vial: 9 Acq On : 30 May 2002 9:56 pm Operator: Morgan Sample : gc/ms scan 5/29 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 31 11:08 2002 Quant Results File :GCMS0520. RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon May 20 15:10:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0528

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.63 178 679898 15.29 ug/1 99 36) Di-n-butylphthalate 27.41 149 959518 16.31 ug/1 99 3 7) Fluoranthene 29.11 202 748861 17.13 ug/1 98 39) Pyrene 29.79 202 772877 18.94 ug/1 92 4 0) Butylbenzylphthalate 31.93 149 366316 17.57 ug/1 92 41) Benzo(a)anthracene 33.42 228 509585 16.73 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.71 149 493648 18.01 ug/1 # 99 43) Chrysene 33.55 228 524141 17.43 ug/1 100 45) Di-n-Octylphthalate 35.45 149 655731 16.04 ug/1 # 90 46) Benzo(b)fluoranthene 36.51 252 419004 15.91 ug/1 97 47) Benzo(k)fluoranthene 36.57 252 458193 16.82 ug/1 97 4 8) Benzo(a)pyrene 37.46 252 302714 12.38 ug/1 96 49) Indeno(1,2,3-cd) pyrene 41.61 276 318780 13.56 ug/1 97 5 0) Dibenz(a,h)anthracene 41.69 278 268619 14.31 ug/1 96 51) Benzo (g, h, Dperylene 42.80 276 287103 15.28 ug/1 96

(#) = qualifier out of range (m) = manual integration REFl.D GCMS0520.M Fri May 31 11:09:51 2002 Page 2

NYC-WTC_000014749

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NYC-WTC_000014749Source: NYC Law Department, mirrored locally

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