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GCMS calibration table June 3, 2002, DEP Labs

Machine-extracted title · confidence 95%

Calibration data table for GCMS analysis containing internal standards and surrogate compounds dated June 3, 2002.

NYC-WTC_000014875–000014882

Folder label: “GCMS X 5/29/02 A 5/31/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAY3102\REF2.D Vial: 5 Acq On : 31 May 2002 3:53 pm Operator: Morgan Sample : gc/ms scan 5/29 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jun 3 9:25 2002 Quant Results File:FGCMS0531.RES *es Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 31 09:43:55 2002 Response via : Initial Calibration DataAcq Meth : GCMS0531

Compound R.T. Qlon Response Cone Unit Qvalue

3 5) Anthracene 25.62 178 672817 15.21 ug/1 100 36) Di-n-butylphthalate 27.41 149 1033742 19.03 ug/1 99 3 7) Fluoranthene 29.11 202 744068 16.52 ug/1 97 39) Pyrene 29.78 202 780695 18.14 ug/1 98 40) Butylbenzylphthalate 31.93 149 357573 16.24 ug/1 97 41) Benzo(a)anthracene 33.42 228 516589 16.36 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.71 149 477755 16.51 ug/1 100 43) Chrysene 33.55 228 550121 17.57 ug/1 99 45) Di-n-Octylphthalate 35.45 149 646342 14.14 ug/1 99 4 6) Benzo(b)fluoranthene 36.51 252 , 434261 16.37 ug/1 97 47) Benzo(k)fluoranthene 36.58 252 437343 15.91 ug/1 100 48) Benzo(a)pyrene 37.47 252 304792 11.89 ug/1 98 49) Indeno(1,2,3-cd)pyrene 41.62 276 345657 14.39 ug/1 99 50) Dibenz(a,h)anthracene 41.69. 278 298685 15.80 ug/1 99 51) Benzo(g,h,i)perylene 42.81 276 310362 15.85 ug/1 99

(#) = qualifier out of range . (m) = manual integration REF2.D GCMS0531.M Mon Jun 03 09:27:24 2002 Page 2

NYC-WTC_0000 14881

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NYC-WTC_000014881Source: NYC Law Department, mirrored locally

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