GCMS calibration table June 3, 2002, DEP Labs

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAY3102\REF2.D Vial: 5 Acq On : 31 May 2002 3:53 pm Operator : Morgan Sample : gc/ms scan 5/29 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jun 3 9:25 2002 Quant Results File:FGCMS0531.RES * w* Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 31 09:43:55 2002 Response via : Initial Calibration DataAcq Meth : GCMS0531

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.07 152 496254 40.00 ug/1 -0.01 10) Naphthalene-d8 15.69 136 1993160 40.00 ug/1 -0.02 17) Acenaphthene-diO 20.99 164 963898 40.00 ug/1 -0.01 30) Phenanthrene-diO 25.42 188 1507942 40.00 ug/1 -0.01 38) Chrysene-dl2 33.47 240 958798 40.00 ug/1 -0.03 44) Perylene-dl2 37.66 264 628535 40.00 ug/1 -0.02

System Monitoring Compounds 28) TCMX 23.14 209 205709 30.85 ug/L -0.01 Spiked Amount 40.000 Recovery 77.13%

Target Compounds Qvalue 2) N-nitrosodimethylamine 5.72 74 146378 9.63 ug/1 100 3) bis(2-Chloroethyl)ether 11.47 93 287268 14.47 ug/1 99 4) 1,3-Dichlorobenzene 11.96 146 258734 13.12 ug/1 99 5) 1,4-Dichlorobenzene 12.11 146 272696 12.77 ug/1 100 6) 1,2-Dichlorobenzene 12.63 146 262538 13.97 ug/1 99 7) 2,2'-oxybis(1-Chioropropan 12.95 45 464225 14.97 ug/1 99 8) N-Nitrosodi-n-propylamine 13.33 70 206983 15.09 ug/1 99 9) Hexachloroethane 13.47 117 86305 10.23 ug/1 98 11) Nitrobenzene 13.75 77 268280 14.58 ug/1 99 12) 1sophorone 14.40 82 588270 17.04 ug/1 99 13) bis(2-Chloroethoxy)methane 15.08 93 344502 15.19 ug/1 99 14) 1,2,4-Trichlorobenzene 15.58 180 216483 14.01 ug/1 99 15) Naphthalene 15.75 128 847397 16.16 ug/1 100 16) Hexachlorobutadiene 16.30 225 80434 11.82 ug/1 98 18) Hexachiorocyclopentadiene 18.49 237 18218 3.08 ug/1 98 19) 2-Chloronaphthalene 19.25 162 438522 17.08 ug/1 100 20) Dimethylphthalate 20.35 163 536768 16.45 ug/1 99 21) 2,6-Dinitrotoluene 20.56 165 112199 15.22 ug/1 99 2 2) Acenaphthylene 20.52 152 682238 14.81 ug/1 99 2 3) Acenaphthene 21.08 153 464457 16.74 ug/1 100 24) 2,4-Dinitrotoluene 21.72 165 138872 16.10 ug/1 98 25) Diethylphthalate 22.48 149 543391 17.98 ug/1 99 26) 4-Chlorophenylphenylether 22.63 204 243797 16.96 ug/1 99 27) Fluorene 22.60 166 515774 18.30 ug/1 99 29) Azobenzene 23.09 77 549141 14.71 ug/L 98 31) N-Nitrosodiphenylamine 23.02 168 185751 16.87 ug/1 96 32) 4-Bromophenylphenylether 24.09 248 123187 16.28 ug/1 97 3 3) Hexachlorobenzene 24.52 284 147516 17.80 ug/1 98 3 4) Phenanthrene 25.49 178 738907 17.43 ug/1 100 (#) = qualifier out of range (m) = manual integration REF2.D GCMS0531.M Mon Jun 03 09:27:23 2002 Page 1

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