GCMS analysis results for sample AE03075, March 5 2002

NYC 9/11 Public Portal Document Library Search Compound Report

: Data File : C:\MSDCHEM\l\5973N\02FEB28\02715.D Vial: 5 Acq On : 28 Feb 2002 1:50 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.94 0.40 ug/L 164070 1,4-Di chlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 42 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 42 3 Pentanol, 5-amino- 103 C5H13NO 002508-29-4 9 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 227 (5.936 min): 02715.D (-) m/z 73.10 100.00% 73

5000 43 P—mTTTPMumtT 5.60 5.80 6.00 6.20 ........ 11.55, , 1.1 87 0- * I “ «‘ I««' ‘ I f ‘ ‘ • I ‘ ‘ ‘ ‘ I • ■ ■111 i ■ • i ■11. । 103 . ।... 11111111 > 111 i ■" ■ i" । IT m/z 43.10 23.02% nz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 11 5.60 5.80 6.00 6.20 43 m/z 45.00 10.00% 27 , 87 113 174 0-TTTTT ■ i ■55 ■ i ■ ■ 118 , । 1uu—un—u—m—emm—nuumn—nmTmg miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 7)3 ■ ■ i ■ ' ' ■ i ■ 1 5.60 5.80 6.0) 6.20 ' ‘ ' 5000 m/z 41.10 9.52% 43 27 55 87 113 174 0- 11"1111 TTTTt ■ i1" ■ i “ ■ ■ T' Tp n1!! ■" ■ | ‘ | "!“' ‘ I ' ‘ " I “‘' I ‘ “ I“ “ I' 1 “I ‘ miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #9904: Pentanol, 5-amino- 33 5.60 5.80 6.00 6.20 m/z 71.00 6.52%

5000

O-TTT t ,...... ................................................................................. .................... ■ ' i ■ ■ ■ ■ i ' ■ ■ ■ i ■ ■ ■ ■ i ■ ■ • ■ i m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

02715.D HP022102.M Fri Mar 01 10:07:07 2002 Page 10

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