GCMS blank sample results, Mar 8 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\FEB2102\LBC.D Vial: 44 Acq On : 23 Feb 2002 11:27 am Operator: Sample : gc/ms scan 1/14 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,2-Benzenedicarboxylic acid, Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

34.01 0.31 ug/1 21028 Chrysene-dl2 33.80

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2 3 4 1,2-Benzenedicarboxylic acid, diiso 390 C24H3804 Bis(2-ethylhexyl) phthalate Phthalic acid, diisooctyl ester 390 C24H3804 390 C24H3804 1,2-Benzenedicarboxylic acid, 3-nit 211 C8H5NO6 Abundance

5000 Scan 3156 (34.012 min): LBC.D (-) 149 1 027554-26-3 86 000117-81-7 78 001330-91-2 64 000603-11-2 56

ux 57 167 41 70 || 84 113 33.60 33.80 34.00 34.20 34.40 i | 207 239 279 -PT m/z 57.00 32.58% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #53134: 1.2-Benzenedicarboxylic acid, diisooctyl ester 149

5000 57 167 33.60 33.80 34.00 34.20 34.40 70 m/z 167.00 30.01% 279

m/z-> ..13104 121132 , J, . • ■ । 40 > । ■ • • • । i • ■ ■ i i • i - I ■ ■ • > । 60 80 100 120 140 • i > ■ ■ ■ i • . ............ 160 180 200 220 240 260 280 , , ,I

Abundance 149

33.60 33.80 34.00 34.20 34.40 5000- m/z 41.05 24.59% 57 167 71 113 IIInIIIv 83 132.......................... ...................27% | m/z-> Abundance 40 60 80 100 120 140 160 180 200 220 #53135: Phthalic acid, diisooctyl ester 149 240 260 280 ... al.... I... 33.60 33.80 34.00 34.20 34.40 i m/z 54.90 20.34%

5000 57 167

m/z-> 71

, il 83 97 113 ' IIaan/n/IuIIIIIIIIIIIIII । ■ 1111 I111 -A 11 v । r 111 40 60 80 100 120 140 160 180 200 220 240 260 280 ....1. v, 33.60 33.80 34.00 34.20 34.40

LBC.D GCMS0208.M Fri Mar 08 09:51:12 2002 Page 4

NYC-WTC_000006270