GCMS surrogate recovery data, Mar 13 2002

NYC 9/11 Public Portal Document LJL aL y ~pulI LCD

Data File : C:\HPCHEM\1\DATA\FEB1502\1943.D Vial: 16 Acq On : 16 Feb 2002 6:00 am Operator: 209 GALOS Sample : re-extract Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 1,2-Benzenedicarboxylic acid, Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

34.01 0.35 ug/1 53092 Chrysene-dl2 33.81

Hit# of 5 Tentative ID MW MolForm CAS# Qual

11, 2-Benzenedicarboxylic acid, 3-nit 211 C8H5NO6 000603-11-2 86 2 Bis(2-ethylhexyl) phthalate 390 C24H3804 000117-81-7 72 3Di-n-octyl phthalate 390 C24H3804 000117-84-0 56 4 Phthalic acid, diisooctyl ester 390 C24H3804m/z149.00 .100.00% 50 001330-91-2 Abundance Scan 3155 (34.010 min): 1943.D (-) 149

5000 167 41 57 71 ................. ........ ,l o TO4 279 33.60 33.80 34.00 34.20 34.40 ,, 83 .118 132 " 11 I | i ■ । । | I । r i' | i i I i । > i' " i ' 207 | ' ' i 1 1 1 ' i ■ ' ' 1 i ' ' 1 ' i 1 ' ■ ■ i ' ■ ' ■ i ' ' m/z 167.00 32.77% m/z-> 40 60) 80 100 120 140 160 180 200 220 240 260 280 Abundance #25513: 1.2-Benzenedicarboxylicacid, 3-nitro- 149

5000- A/ 33.60 33.80 34.00 34.20 34.40 167 71 m/z 57.00 28.63% i 83 113 .02 ---------------------- m/z-__ 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance 149

33.60 33.80 34.00 34.20 34.40 5000- m/z 41.05 24.69% 57 167 71 83 113 279 132 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #53129: Di-n-octyl phthalate ........... ...................... ........................... 149 33.60 33.80 34.00 34.20 34.40 m/z 43.05 23.89% 5000 167 31 57 70 108

m/z-> 40 60 80 100 in.. L. 120 140 160 IaaI*IIIIIIIuanIuIIIgum 180 200 220 240 260 280 M 33.60 33.80 34.00 34.20 34.40

1943.D GCMS0208.M Fri Mar 08 16:14:40 2002 Page 2

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