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GCMS calibration results for PAHs, Feb 2002

Machine-extracted title · confidence 95%

Calibration data for polycyclic aromatic hydrocarbons and deuterated standards analyzed on February 15, 2002.

NYC-WTC_000005849–000005851

Folder label: “GCMS X 2/11/02 A 2/15/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\FEB14O2\REF1.D Vial: 24 Acq On : 15 Feb 2002 1:32 am Operator: 209 GALOS Sample : GC/MS SCAN 2/11 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 15 11:45 2002 (Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.32 168 74426 (3090-ug/1 99 31) 4-Bromophenyl-phenylether 24.41 248 57673 4.67 ug/1 98 32) Hexachlorobenzene 24.84 284 69334 •4.80 ug/1 97 33) Phenanthrene 25.82 178 287929 <4.89 ug/1 100 34) Anthracene 25.95 178 260550 4.52 ug/1 99 35) Di-n-butylphthalate 27.71 149 419668 5.10 ug/1 99 36) Fluoranthene 29.45 202 288336 4.90 ug/1 100 3 9) Pyrene 30.13 202 301130 (4.0ug/l 100 40) Butylbenzylphthalate 32.25 149 127675 /3.60 ug/1 96 41) Benzo(a)anthracene 33.76 228 226238 '4.83 ug/1 99 42) Bis(2-ethylhexyl)phthalate 34.03 149 185025 3.86 ug/1 98 43) Chrysene 33.89 228 248760 5.40 ug/1 99 45) Di-n-Octylphthalate 35.77 149 203514 Q:74ug/1 # 98 46) Benzo(b)fluoranthene 36.89 252 191068 4 4.56 ug/1 99 47) Benzo(k)fluoranthene 36.96 252 214304 <5.09 ug/1 99 48) Benzo(a)pyrene 37.90 252 141995 4.09 ug/1 100 49) Indeno(1,2,3-cd)pyrene 42.32 276 137776 35 ug/1 99 50) Dibenz(a,h)anthracene 42.39 278 122433 5.06 ug/1 98 51) Benzo(g,h,i)perylene 43.58 276 126654 4.96 ug/1 97

(#) = qualifier out of range (m) = manual integration REFI.D GCMS0208.M Fri Feb 15 11:48:49 2002 Page 2

NYC-WTC_000005850

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NYC-WTC_000005850Source: NYC Law Department, mirrored locally

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