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GCMS calibration results for sample AE00109, Feb 2002

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Calibration report listing recovery percentages for volatile organic compounds in sample AE00109 on February 14, 2002.

NYC-WTC_000005833–000005836

Folder label: “GCMS X 2/11/02 A 2/15/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\FEB1402\CAL10.D Vial: 2 Acq On : 14 Feb 2002 11:36 pm Operator: 209 GALOS Sample : GC/MS SCAN 2/11 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 15 11:40 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.33 168 246679 9.46 ug/1 99 31) 4-Bromophenyl-phenylether 24.41 248 156641 9.29 ug/1 99 32) Hexachlorobenzene 24.85 284 188418 9.54 ug/1 99 33) Phenanthrene 25.82 178 753743 9.37 ug/1 100 34) Anthracene 25.96 178 731602 9.28 ug/1 100 35) Di-n-butylphthalate 27.71 149 1028224 9.15 ug/1 99 36) Fluoranthene 29.45 202 756180 9.42 ug/1 97 3 9) Pyrene 30.13 202 781040 9.01 ug/1 97 40) Butylbenzylphthalate 32.25 149 403368 8.41 ug/1 96 41) Benzo(a)anthracene 33.77 228 582215 9.19 ug/1 100 42) Bis(2-ethylhexyl)phthalate 34.03 149 495233 (7.64-ug/1 99 43) Chrysene 33.90 228 583243 9.36 ug/1 99 45) Di-n-Octylphthalate 35.77 149 698660 6.96 ug/1 # 98 46) Benzo(b)fluoranthene 36.89 252 505274 8.91 ug/1 100 47) Benzo(k)fluoranthene 36.97 252 518606 9.10 ug/1 99 48) Benzo(a)pyrene 37.91 252 436750 9.30 ug/1 100 49) Indeno(1,2,3-cd)pyrene 42.33 276 420008 9.80 ug/1 98 50) Dibenz(a,h)anthracene 42.41 278 326293 9.96 ug/1 99 51) Benzo(g,h,i)perylene 43.60 276 343731 9.94 ug/1 99

(#) = qualifier out of range (m) = manual integration CAL10.D GCMS0208.M Fri Feb 15 11:43:47 2002 Page 2

NYC-WTC_000005835

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NYC-WTC_000005835Source: NYC Law Department, mirrored locally

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