GCMS calibration results for sample AE00109, Feb 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\FEB1402\CAL10.D Vial: 2 Acq On : 14 Feb 2002 11:36 pm Operator: 209 GALOS Sample : GC/MS SCAN 2/11 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 15 11:40 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.35 152 424560 20.00 ug/1 0.00 10) Naphthalene-d8 15.99 136 1689561 20.00 ug/1 0.00 17) Acenaphthene-diO 21.30 164 918241 20.00 ug/1 0.00 29) Phenanthrene-dlO 25.76 188 1330124 20.00 ug/1 0.00 38) Chrysene-dl2 33.84 240 989440 20.00 ug/1 0.00 44) Perylene-dl2 38.11 264 627137 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 0.00 235 Od 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds d -/2 Qvalue 2) N-nitroso-dimethyl amine 5.96 74 166841 9.82 ug/1 98 3) bis(2-Chloroethyl)ether 11.76 93 286524 10.27 ug/1 99 4) 1,3-Dichlorobenzene 12.25 146 323653 9.74 ug/1 98 5) 1,4-Dichlorobenzene 12.39 146 337337 9.96 ug/1 98 6) 1,2-Dichlorobenzene 12.91 146 323166 10.05 ug/1 100 7) 2,2'-oxybis(1-Chloropropan 13.23 45 455384 10.78 ug/1 98 8) N-Nitroso-di-n-propylamine 13.62 70 210039 10.52 ug/1 97 9) Hexachioroethane 13.76 117 132056 9.75 ug/1 97 11) Nitrobenzene 14.04 77 335924 9.67 ug/1 96 12) Isophorone 14.68 82 580501 9.89 ug/1 100 13) bis(2-Chloroethoxy)methane 15.36 93 348930 9.55 ug/1 98 14) 1,2,4-Trichlorobenzene 15.88 180 275530 9.53 ug/1 97 15) Naphthalene 16.05 128 858288 9.54 ug/1 100 16) Hexachlorobutadiene 16.59 225 166026 9.60 ug/1 98 18) Hexachlorocyclopentadiene 18.79 237 87753 6.68 ug/1 98 19) 2-Chloronaphthalene 19.56 162 515762 9.42 ug/1 99 20) Dimethylphthalate 20.64 163 615083 9.65 ug/1 99 21) 2,6-Dinitrotoluene 20.86 165 134682 9.32 ug/1 98 22) Acenaphthylene 20.84 152 747038 9.45 ug/1 99 2 3) Acenaphthene 21.40 153 529791 9.58 ug/1 100 24) 2,4-Dinitrotoluene 22.04 165 171817 9.39 ug/1 98 25) Diethylphthalate 22.79 149 635576 9.59 ug/1 99 26) 4-Chlorophenyl-phenylether 22.94 204 277548 9.73 ug/1 99 27) Fluorene 22.92 166 572755 9.49 ug/1 100 28) Azobenzen/ 1,2-Diphenylhyd 23.41 77 654820 9.39 ug/L 98

(#) = qualifier out of range (m) = manual integration CAL10.D GCMS0208.M Fri Feb 15 11:43:43 2002 Page 1

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