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GCMS reference standard results, sample AE00109, Feb 2002

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Laboratory report listing recovery percentages for thirteen volatile organic compounds in reference standard AE00109 analyzed on February 14, 2002.

NYC-WTC_000005837–000005841

Folder label: “GCMS X 2/11/02 A 2/15/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\FEB1402\REF2.D Vial: 25 Acq On : 15 Feb 2002 2:30 am Operator: 209 GALOS Sample : GC/MS SCAN 2/11 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 15 11:49 2002 <Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.32 168 98458 (400 ug/1 98 31) 4-Bromophenyl-phenylether 24.41 248 74003 • 4.6 6 ug/1 96 3 2) Hexachiorobenzene 24.84 284 88142 /4.73 ug/1 98 33) Phenanthrene 25.82 178 369551 4.87 ug/1 100 34) Anthracene 25.95 178 340887 (4.59 ug/1 99 35) Di-n-butylphthalate 27.71 149 555229 5.24 ug/1 99 36) Fluoranthene 29.45 202 365003 4.82 ug/1 99 3 9) Pyrene 30.12 202 380166 (4.6% ug/1 97 40) Butylbenzylphthalate 32.25 149 167276 ‘3.70 ug/1 96 41) Benzo(a)anthracene 33.76 228 290692 4.87 ug/1 99 42) Bis(2-ethylhexyl)phthalate 34.02 149 248499 4.07 ug/1 97 43) Chrysene 33.89 228 311770 (5.31 ug/1 99 45) Di-n-Octylphthalate 35.76 149 279566 95 46) Benzo(b)fluoranthene 36.88 252 272094 ‘4, 95 ug/1 99 47) Benzo(k)fluoranthene 36.96 252 289443 (5.24 ug/1 99 48) Benzo(a)pyrene 37.90 252 187064 <5710 ug/1 99 49) Indeno(1,2,3-cd)pyrene 42.32 276 187443 4.50 ug/1 99 50) Dibenz(a,h)anthracene 42.39 278 162077 5.10 ug/1 99 51) Benzo(g,h,i)perylene 43.59 276 164377 4.90 ug/1 96

(#) = qualifier out of range (m) = manual integration REF2.D GCMS0208.M Fri Feb 15 11:52:03 2002 Page 2

NYC-WTC_000005840

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NYC-WTC_000005840Source: NYC Law Department, mirrored locally

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