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GCMS reference results for sample AD31662, Feb 2002

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Reference analysis report showing measured concentrations of volatile organic compounds in sample AD31662 on February 13, 2002.

NYC-WTC_000005751–000005755

Folder label: “GCMS X 2/11/02 A 2/13/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\FEB1302\REF.D Vial: 4 Acq On : 13 Feb 2002 6:08 pm Operator: 209 GALOS Sample : GC/MS SCAN 2/11 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 15 9:50 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.32 168 71515 4.69 ug/1 100 31) 4-Bromophenyl-phenylether 24.41 248 52514 5.33 ug/1 99 32) Hexachlorobenzene 24.84 284 65222 5.65 ug/1 96 3 3) Phenanthrene 25.82 178 264535 5.63 ug/1 100 34) Anthracene 25.95 178 239615 5.20 ug/1 99 35) Di-n-butylphthalate 27.71 149 374385 5.70 ug/1 99 36) Fluoranthene 29.45 202 264348 5.63 ug/1 100 3 9) Pyrene 30.13 202 277957 5.65 ug/1 99 40) Butylbenzylphthalate 32.25 149 117354 4.31 ug/1 93 41) Benzo(a)anthracene 33.77 228 206690 5.74 ug/1 99 42) Bis(2-ethylhexyl)phthalate 34.03 149 168722 4.58 ug/1 98 43) Chrysene 33.90 228 225698 6.37 ug/1 100 45) Di-n-Octylphthalate 35.77 149 178124 3.09 ug/1 # 97 46) Benzo(b)fluoranthene 36.89 252 183900 5.66 ug/1 99 47) Benzo(k)fluoranthene 36.96 252 209900 6.43 ug/1 98 48) Benzo(a)pyrene 37.90 252 128201 4.76 ug/1 99 49) Indeno(1,2,3-cd)pyrene 42.33 276 130702 5.32 ug/1 98 50) Dibenz(a,h)anthracene 42.40 278 111903 5.95 ug/1 99 51) Benzo(g,h,i)perylene 43.59 276 120253 6.07 ug/1 98

(#) = qualifier out of range (m) = manual integration REF.D GCMS0208.M Fri Feb 15 09:52:54 2002 Page 2

NYC-WTC_000005754

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NYC-WTC_000005754Source: NYC Law Department, mirrored locally

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