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GCMS calibration data file for sample GC/MS SCAN 1/15, Feb

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Instrument data file from February 2002 listing retention times and concentrations for polycyclic aromatic hydrocarbon surrogates.

NYC-WTC_000052575–000052577

Folder label: “GCMS X 1/15/02 A 2/28/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\FEB1402\REF.D Vial: 4 Acq On : 14 Feb 2002 11:36 am Operator: 209 GALOS Sample : GC/MS SCAN 1/15 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 19 12:34 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.32 168 36134 (1.87g/ 1 97 31) 4-Bromophenyl-phenylether 24.40 248 29362 2.36 ug/1 98 32) Hexachlorobenzene 24.84 284 33750 (203Duq/1 97 33) 34) Phenanthrene Anthracene 25.82 25.94 178 178 145520 130897 (2.45 g/1 (2.25 g/1 100 99 35) Di-n-butylphthalate 27.72 149 175300 (2.1Dug/1 99 36) Fluoranthene 29.44 202 137279 2.31 ug/1 99 39) Pyrene 30.12 202 145499 2.39ug/1 99 40) Butylbenzylphthalate 32.25 149 51435 1.53 ug/1 98 41) Benzo(a)anthracene 33.77 228 107136 2.41 ug/1 99 42) Bis(2-ethylhexyl)phthalate 34.02 149 67909 (1.49 ug/1 98 43) Chrysene 33.89 228 123289 (.82 ug/1 99 45) Di-n-Octylphthalate 35.77 149 66195 0.92 ug/1 # 98 46) Benzo(b)fluoranthene 36.89 252 93473 2.30 ug/1 99 47) Benzo(k)fluoranthene 36.95 252 112017 2.75 ug/1 99 48) Benzo(a)pyrene 37.90 252 63630 1.89 ug/1 98 49) Indeno(1,2,3-cd)pyrene 42.32 276 64941 2.12 ug/1 94 50) Dibenz(a,h)anthracene 42.39 278 57508 2.45 ug/1 100 51) Benzo(g,h,i)perylene 43.59 276 61786 2.50 ug/1 98

(#) = qualifier out of range (m) = manual integration REF.D GCMS0308.M Thu Mar 14 15:21:54 2002 Page 2

NYC-WTC_000052576

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NYC-WTC_000052576Source: NYC Law Department, mirrored locally

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