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GCMS reference results for sample AD30643, Dec 2001

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Reference analysis report showing measured concentrations of volatile organic compounds in sample AD30643 on December 30, 2001.

NYC-WTC_000005781–000005785

Folder label: “GCMS X 2/11/02 A 2/13/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\FEB1302\REFA.D Vial: 5 Acq On : 13 Feb 2002 7:07 pm Operator: 209 GALOS Sample : GC/MS SCAN 2/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 15 9:55 2002 (Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.32 168 74674 4.52 ug/1 99 31) 4-Bromophenyl-phenylether 24.41 248 54617 5.11 ug/1 97 32) Hexachlorobenzene 24.85 284 65887 5.27 ug/1 96 3 3) Phenanthrene 25.82 178 282008 5.53 ug/1 100 3 4) Anthracene 25.95 178 259239 5.19 ug/1 99 35) Di-n-butylphthalate 27.71 149 418124 5.87 ug/1 99 36) Fluoranthene 29.45 202 289943 5.70 ug/1 99 3 9) Pyrene 30.13 202 301923 5.45 ug/1 100 40) Butylbenzylphthalate 32.25 149 129611 4.23 ug/1 94 41) Benzo(a)anthracene 33.77 228 234345 5.79 ug/1 100 42) Bis(2-ethylhexyl)phthalate 34.03 149 183359 4.43 ug/1 99 43) Chrysene 33.90 228 253349 6.36 ug/1 99 45) Di-n-Octylphthalate 35.77 149 203428 3.10 ug/1 # 96 46) Benzo(b)fluoranthene 36.89 252 205624 5.55 ug/1 100 47) Benzo(k)fluoranthene 36.96 252 241918 6.50 ug/1 99 48) Benzo(a)pyrene 37.90 252 144180 4.69 ug/1 99 49) Indeno (1,2,3-cd) pyrene 42.33 276 154208 5.50 ug/1 99 50) Dibenz(a,h)anthracene 42.40 278 133408 6.23 ug/1 99 51) Benzo(g,h,i)perylene 43.59 276 140916 6.23 ug/1 98

(#) = qualifier out of range (m) = manual integration REFA.D GCMS0208.M Fri Feb 15 09:57:52 2002 Page 2

NYC-WTC_000005784

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NYC-WTC_000005784Source: NYC Law Department, mirrored locally

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