GCMS reference results for sample AD30643, Dec 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\FEB1302\REFA.D Vial: 5 Acq On : 13 Feb 2002 7:07 pm Operator: 209 GALOS Sample : GC/MS SCAN 2/11 Inst : GC/MS 209 Mise : . Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 15 9:55 2002 1Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update Response via : : Wed Feb 13 11:43:23 2002 Initial Calibration 1 O /

DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.34 152 270403 20.00 ug/1 0.00 10) Naphthalene-d8 15.99 136 1035249 20.00 ug/1 0.00 17) Acenaphthene-diO 21.30 164 559906 20.00 ug/1 0.00 29) Phenanthrene-diO 25.76 188 842879 20.00 ug/1 0.00 38) Chrysene-dl2 33.83 240 632223 20.00 ug/1 -0.02 44) Perylene-dl2 38.11 264 410080 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 30.83 235 43972 5.20 ug/mL 0.34 Spiked Amount 5.000 Recovery = 104.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.96 74 36868 3.41 ug/1 99 3) bis(2-Chloroethyl)ether 11.74 93 89235 5.02 ug/1 99 4) 1,3-Dichlorobenzene 12.24 146 69711 3.30 ug/1 99 5) 1,4-Dichlorobenzene 12.39 146 74188 3.44 ug/1 99 6) 1,2-Dichlorobenzene 12.90 146 73570 3.59 ug/1 99 7) 2,21-oxybis(1-Chloropropan 13.23 45 142182 5.28 ug/1 99 8) N-Nitroso-di-n-propylamine 13.61 70 70651 5.56 ug/1 95 9) Hexachloroethane 13.76 117 22942 2.66 ug/1 99 11) Nitrobenzene 14.02 77 94435 4.44 ug/1 96 12) 1sophorone 14.68 82 202664 5.64 ug/1 99 13) bis(2-Chloroethoxy)methane 15.36 93 115462 5.16 ug/1 99 14) 1,2,4-Trichlorobenzene 15.87 180 65486 3.70 ug/1 99 15) Naphthalene 16.04 128 238554 4.33 ug/1 99 16) Hexachlorobutadiene 16.59 225 26125 2.46 ug/1 99 18) Hexachlorocyclopentadiene 18.79 237 3073 0.38 ug/1 90 19) 2-Chloronaphthalene 19.55 162 147045 4.40 ug/1 99 20) Dimethylphthalate 20.64 163 236014 6.07 ug/1 99 21) 2,6-Dinitrotoluene 20.86 165 38888 4.41 ug/1 99 22) Acenaphthylene 20.84 152 234230 4.86 ug/1 99 23) Acenaphthene 21.40 153 168510 5.00 ug/1 99 24) 2,4-Dinitrotoluene 22.03 165 49762 4.46 ug/1 96 25) Diethylphthalate 22.77 149 240752 5.96 ug/1 100 26) 4-Chlorophenyl-phenylether 22.94 204 91101 5.24 ug/1 99 27) Fluorene 22.92 166 190811 5.19 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.40 77 227730 5.36 ug/L 96

(#) = qualifier out of range (m) = manual integration REFA.D GCMS0208.M Fri Feb 15 09:57:49 2002 Page 1

NYC-WTC_000005783